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@ARTICLE{Vasylyev:154049,
author = {Vasylyev, Olexsandr and Brychevskyi, Mykola and
Brodnikovskyi, Iegor and Firstov, Sergiy and Andrzejczuk,
Mariusz and Spychalski, Maciek and Lewandowska, Malgorzata
and Kurzydlowski, Krzysztof Jan and Steinberger-Wilckens,
Robert and Mertens, Josef and Malzbender, Jürgen},
title = {{N}ucleation and {G}rowth {M}echainsms of {Z}irconia {F}ilm
{D}eposited on {P}orous {N}ickel {O}xide - {Z}irconia
{S}ubstrate by {E}lectron {B}eam - {P}hysical {V}apor
{D}eposition},
journal = {Advances in Ceramic Science and Engineering},
volume = {3},
number = {2014},
issn = {2325-5129},
address = {Riley, Ind.},
publisher = {Science and Engineering Publishing Company (SEP)},
reportid = {FZJ-2014-03457},
pages = {25-35},
year = {2014},
abstract = {The structure of the transitional zone between a zirconia
film deposited by EB-PVD and its porous NiO-ZrO2 substrate
were studied using transmission and scanning electron
microscopy. The plausible condensation mechanisms of
zirconia from its vapor phase onto zirconia and nickel oxide
phases of the substrate were established. The condensation
of zirconia was identified as a two-stage process with two
mechanisms of growth, planar and cellular, similar to
solidification from the liquid phase. ZrO2 condensation on
ZrO2 and NiO phases occurs with different routes. During the
planar growth on the ZrO2, the ZrO2 film nucleates and grows
up to ~0.3-0.5 μm with no orientation preference as
continuous "layer by layer" defective film. The planar ZrO2
film on the NiO of ~0.5-0.7 μm thickness is discontinuous
and porous; it consists of oriented structurally perfect
"islands". The differences found are probably the result of
differences in the melting temperature of ZrO2 and NiO, and
Zr and Ni affinities to oxygen as well as their different
behavior under high vacuum. The deposition affected zone
surrounding the ZrO2 nucleation site is
established.Keywords: Zirconia Film; Nucleation Mechanism;
Growth Mechanism; Thin Structure; Solid Oxide Fuel Cell;
Electron Beam – Physical Vapor Deposition},
cin = {IEK-9 / IEK-2},
ddc = {670},
cid = {I:(DE-Juel1)IEK-9-20110218 / I:(DE-Juel1)IEK-2-20101013},
pnm = {123 - Fuel Cells (POF2-123) / 152 - Renewable Energies
(POF2-152)},
pid = {G:(DE-HGF)POF2-123 / G:(DE-HGF)POF2-152},
typ = {PUB:(DE-HGF)16},
url = {https://juser.fz-juelich.de/record/154049},
}