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@ARTICLE{Mcke:154957,
      author       = {Mücke, R. and Büchler, O. and Menzler, N. H. and Lindl,
                      B. and Vaßen, R. and Buchkremer, H. P.},
      title        = {{H}igh-precision green densities of thick films and their
                      correlation with powder, ink, and film propertiesfuel cell},
      journal      = {Journal of the European Ceramic Society},
      volume       = {34},
      number       = {15},
      issn         = {0955-2219},
      address      = {Amsterdam [u.a.]},
      publisher    = {Elsevier Science},
      reportid     = {FZJ-2014-04166},
      pages        = {3897 - 3916},
      year         = {2014},
      abstract     = {A precise geometrical method employing optical profilometry
                      for green density measurements of thick films is presented
                      that provides a typical reproducibility of $0.1–0.2\%$
                      theoretical density (TD) and a measurement uncertainty of
                      $0.2–0.4\%$ TD for layer thicknesses of around 50 μm. The
                      procedure can be applied for all thick films with a dried
                      thickness of 10 μm or greater. In a case study, the green
                      densities of screen-printed zirconia layers were
                      investigated as a function of the starting powders (grain
                      sizes from 0.1 to 0.4 μm), the solid content, the chain
                      length of ethyl cellulose as binder and its concentration,
                      and two different dispersants and their concentration.
                      Rheological ink properties, surface roughness, drying
                      stresses from deflection measurements, the mechanical
                      properties of green films, and the equivalent compaction
                      pressure were measured and correlated with the green density
                      data. Compressive binder forces and lubrication effects
                      dominated the packing of the particles.},
      cin          = {IEK-1},
      ddc          = {660},
      cid          = {I:(DE-Juel1)IEK-1-20101013},
      pnm          = {123 - Fuel Cells (POF2-123) / SOFC - Solid Oxide Fuel Cell
                      (SOFC-20140602)},
      pid          = {G:(DE-HGF)POF2-123 / G:(DE-Juel1)SOFC-20140602},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000340976200052},
      doi          = {10.1016/j.jeurceramsoc.2014.04.012},
      url          = {https://juser.fz-juelich.de/record/154957},
}