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001     155849
005     20240619083501.0
024 7 _ |a 10.1063/1.4881796
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024 7 _ |a 1089-7623
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024 7 _ |a 0034-6748
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024 7 _ |a WOS:000339010500062
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037 _ _ |a FZJ-2014-04807
041 _ _ |a English
082 _ _ |a 530
100 1 _ |a Pfleiderer, P.
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245 _ _ |a X-ray scattering in the vorticity direction and rheometry from confined fluids
260 _ _ |a London
|c 2014
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336 7 _ |a Journal Article
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336 7 _ |a article
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520 _ _ |a An X-ray flexure-based microgap rheometer (X-FMR) has been designed for combining rheology and in situ small-angle X-ray scattering from the vorticity plane. The gap distance can be varied continuously from 500 μm down to several μm, which provides the unique possibility to generate a strong confinement for many complex fluids. A singular advantage of this setup is the possibility to directly probe the vorticity direction of the flow field with a microfocus X-ray beam and to probe the structural response of the fluid to combined shear and confinement in the vorticity plane. The sliding-plate setup operates over a wide range of shear rates of γ̇ = 10−3–103 s−1 and strains in the range of 10−4–102. The flexure-based bearing maintains the plate parallelism within 10−5 rad. The X-FMR requires very small sample volumes on the order of 10 μl. The applicability of the device is demonstrated here with limited examples of a nematic suspension of fd virus (rods), and a crystalline suspension containing sterically stabilized polystyrene-butylacrylate latex particles.
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700 1 _ |a Baik, S. J.
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700 1 _ |a Zhang, Z.
|0 P:(DE-HGF)0
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700 1 _ |a Vleminckx, G.
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700 1 _ |a Lettinga, M.P.
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700 1 _ |a Grelet, E.
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700 1 _ |a Vermant, J.
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700 1 _ |a Clasen, C.
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773 _ _ |a 10.1063/1.4881796
|g Vol. 85, no. 6, p. 065108 -
|0 PERI:(DE-600)2105249-9
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|p 065108
|t Journal of scientific instruments
|v 85
|y 2014
|x 0950-7671
856 4 _ |u https://juser.fz-juelich.de/record/155849/files/FZJ-2014-04807.pdf
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910 1 _ |a Forschungszentrum Jülich GmbH
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