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000015642 0247_ $$2DOI$$a10.1016/j.jeurceramsoc.2011.03.035
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000015642 084__ $$2WoS$$aMaterials Science, Ceramics
000015642 1001_ $$0P:(DE-Juel1)VDB88648$$aYoon, S.$$b0$$uFZJ
000015642 245__ $$aSpark plasma sintering of nanocrystalline BaTiO3-powders: Consolidation behavior and dielectric characteristics
000015642 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2011
000015642 300__ $$a1723 - 1731
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000015642 440_0 $$03891$$aJournal of the European Ceramic Society$$v31$$x0955-2219$$y9
000015642 500__ $$3POF3_Assignment on 2016-02-29
000015642 500__ $$aThis work was supported by the Korea Research Foundation Grant funded by the Korean Government (KRF-2007-D00124). S. Yoon acknowledges support from COST Action 539 (COST-STSM-539-03589) of the European Union. NAMICS Corporation, Niigata (Japan) is gratefully acknowledged for financial support within a common collaboration project. The authors are grateful to Dr. Wessel Egbert for FE-SEM and to Dr. Detlev Hennings for helpful discussion and comments.
000015642 520__ $$aBaTiO3 nanopowders prepared by two different wet chemical routes, one based on microemulsion-mediated synthesis (M-BT) and the other one on the alkoxide-hydroxide method (A-BT) were consolidated by spark plasma sintering (SPS). The densification process, the linear shrinkage rates and the relative densities achieved were strongly dependant on the synthetic route. The results show that fully densified BaTiO3 ceramics with a grain size of about 200 nm can be obtained in both cases by controlling the sintering temperature during the SPS process. The study of dielectric properties revealed that M-BT derived ceramics show higher permittivity values compared to those obtained for A-BT. The influence of the barium/titanium ratio on the sintering behavior and the dielectric properties is discussed. (C) 2011 Elsevier Ltd. All rights reserved.
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000015642 65320 $$2Author$$aBaTiO3
000015642 65320 $$2Author$$aSpark plasma sintering
000015642 65320 $$2Author$$aGrain growth
000015642 65320 $$2Author$$aDielectric properties
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