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@ARTICLE{Schneller:15643,
author = {Schneller, T. and Halder, S. and Waser, R. and Pithan, C.
and Dornseiffer, J. and Shiratori, Y. and Houben, L. and
Vyshnavi, N. and Majumber, S.B.},
title = {{N}anocomposite thin films for miniaturized multi-ayer
ceramic capacitors prepared from barium titanate
nanoparticle based hybrid solutions},
journal = {Journal of materials chemistry},
volume = {21},
issn = {0959-9428},
address = {London},
publisher = {ChemSoc},
reportid = {PreJuSER-15643},
pages = {7953 - 7965},
year = {2011},
note = {The research described in this publication was supported by
the Deutsche Forschungsgemeinschaft within the priority
program SPP1181. S. B. Majumder wishes to thank Alexander
von Humboldt foundation for the partial financial support to
carry out the research work and N. Vyshnavi acknowledges the
financial support rendered by the DAAD sandwich Fellowship.
Thomas Possinger is acknowledged for preparing the artwork.},
abstract = {In the present work a flexible approach for the wet
chemical processing of nanocomposite functional thin films
is demonstrated. Barium titanate (BTO) based nanocomposite
thin films for future miniaturized multi-layer ceramic
capacitors are chosen as model systems to introduce the
concept of "hybrid solutions" which consist of stabile
mixtures of reverse micelle derived BTO nanoparticle
dispersions and conventional molecular precursor solutions
of either the same (BTO:BTO) or a specifically different
material such as zirconia (BTO:ZrO2). While in the case of
using BTO:BTO hybrid solutions an interesting mode of
microstructure control is found, the use of BTO:ZrO2 hybrid
solutions with various BTO : ZrO2 ratios leads to
nanocomposite films. BTO:BTO hybrid solutions yield columnar
grown films with excellent permittivities up to 1050 with a
significantly reduced number of coating steps at 700 degrees
C. Low values of the temperature coefficient of capacitance
are realized in the BTO-ZrO2 nanocomposite thin films. The
observed dielectric behavior of these films is explained
based on the formation of a core-shell type microstructure
on the nanoscale. A detailed high resolution transmission
electron microscopy study combined with Raman spectroscopy
and X-ray diffraction gives evidence for the proposed
BTO-ZrO2 nanocomposite character of these thin films.},
keywords = {J (WoSType)},
cin = {JARA-FIT / PGI-7 / IEK-8},
ddc = {540},
cid = {$I:(DE-82)080009_20140620$ / I:(DE-Juel1)PGI-7-20110106 /
I:(DE-Juel1)IEK-8-20101013},
pnm = {Grundlagen für zukünftige Informationstechnologien /
Atmosphäre und Klima},
pid = {G:(DE-Juel1)FUEK412 / G:(DE-Juel1)FUEK491},
shelfmark = {Chemistry, Physical / Materials Science, Multidisciplinary},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000290912900017},
doi = {10.1039/c1jm10607d},
url = {https://juser.fz-juelich.de/record/15643},
}