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@PHDTHESIS{Kronenberg:15864,
      author       = {Kronenberg, U.},
      title        = {{S}ynthesis and radiofluorination of putative {NMDA}
                      receptor ligands},
      volume       = {4338},
      school       = {Univ. Köln},
      type         = {Dr. (Univ.)},
      address      = {Jülich},
      publisher    = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
      reportid     = {PreJuSER-15864, Juel-4338},
      series       = {Berichts des Forschungszentrums Jülich},
      pages        = {III, 95 p.},
      year         = {2010},
      note         = {Record converted from JUWEL: 18.07.2013; Köln, Univ.,
                      Diss., 2010},
      abstract     = {In the course of this work on the synthesis of radioligands
                      for the NMDA receptor the authentic standards and labeling
                      precursors of four compounds with an amidine structure was
                      performed. Synthesis of the precursors followed reaction
                      conditions given in the literature and was successful. The
                      imidoesters used for the synthesis were obtained from their
                      nitriles in a Pinner synthesis, while 2-hydroxybenzylamine
                      was synthesized in a reduction of 2-hydroxybenzonitrile
                      using borane as a reducing agent. After a coupling reaction
                      of the amine and the imidoester in DMF using triethylamine
                      as base the precursors were obtained in good yields and
                      purified by crystallization from methanol. The cyclic
                      standard compound was synthesized directly from
                      2-(bromomethyl)- benzonitrile and 2-hydroxybenzylamine in a
                      ring closing reaction. Similar to the other precursors,
                      crystallization from methanol produced a pure compound....},
      cin          = {INM-5},
      ddc          = {500},
      cid          = {I:(DE-Juel1)INM-5-20090406},
      pnm          = {Funktion und Dysfunktion des Nervensystems},
      pid          = {G:(DE-Juel1)FUEK409},
      typ          = {PUB:(DE-HGF)11 / PUB:(DE-HGF)3},
      url          = {https://juser.fz-juelich.de/record/15864},
}