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@PHDTHESIS{Weiss:16436,
author = {Weiss, Christian},
title = {{STM} beyond vacuum tunnelling, a route to ultra high
resolution},
volume = {47},
type = {Dr. (FH)},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {PreJuSER-16436},
isbn = {978-3-89336-813-6},
series = {Schriften des Forschungszentrums Jülich.
Schlüsseltechnologien / Key Technologies},
year = {2011},
note = {Record converted from VDB: 12.11.2012},
abstract = {Direct imaging is a fast and reliable method for the
characterization of surfaces. When it comes to small surface
structures in the size of the features e.g. in todays
computer processors, classical optical imaging methods fail
in resolving these structures. With the invention of the
scanning tunnelling microscope (STM) for the first time it
became possible to image the structure of surfaces with
atomic precision. However, the STM fails in resolving
complex chemical structures like e.g. organic molecules. The
lack of chemical sensitivity in STM images can be overcome
by the condensation of molecular hydrogen or deuterium in
the STM junction. Images recorded in the so-called scanning
tunnelling hydrogen microscopy (STHM) closely resemble the
chemical structure of different organic molecules. However,
the mechanism behind the contrast formation has not been
addressed so far. Here we show that the origin of the STHM
contrast is a single hydrogen (H$_{2}$) or deuterium
(D$_{2}$) molecule located directly below the tip apex that
acts as a combined sensor and signal transducer. Together
with the tip the gas molecule forms a nano-scale force
sensor, comparable to sensors in atomic force microscopy
(AFM), which probes the total electron density (TED) of the
surface trough the Pauli repulsion and converts this signal
into variations of the junctions’ conductance again via
Pauli repulsion. Other than the sensors in conventional
scanning force techniques, due to its size, the sensor of
the STHM junction is intrinsically insensitive to long-range
forces, usually limiting the image resolution. The
insensitivity to long-range forces results in a high image
resolution, so that even small changes in the TED leave a
mark in obtained STHM images. The resolution hereby reaches
an unprecedented level as can be seen by the direct imaging
of local intermolecular interactions like e.g. hydrogen
bonds appear with remarkable clarity in STHM images of
organic layers. Thus, besides the identification of chemical
species of different adsorbates, the STHM mode allows the
study of interactions between adsorbates which e.g. lead to
their self organization on the surface. Therefore, the STHM
mode may give important insight in the driving mechanisms
behind the formation and composition of matter on the atomic
level. However, the STHM mode, in which a single H$_{2}$
(D$_{2}$) molecule probes the TED of the surface, is only
one example of a broader class of sensors. It is
conceivable, that by an appropriate choice of the molecule
in the junction, other surface properties can be imaged
which are usually inaccessible by other imaging techniques.},
cin = {PGI-3 / JARA-FIT},
cid = {I:(DE-Juel1)PGI-3-20110106 / $I:(DE-82)080009_20140620$},
pnm = {Grundlagen für zukünftige Informationstechnologien},
pid = {G:(DE-Juel1)FUEK412},
typ = {PUB:(DE-HGF)11 / PUB:(DE-HGF)3},
url = {https://juser.fz-juelich.de/record/16436},
}