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000171712 0247_ $$2doi$$a10.1016/j.matlet.2014.05.121
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000171712 245__ $$aSpray-drying synthesis of Na$_{2}$FePO$_{4}$F/carbon powders for lithium-ion batteries
000171712 260__ $$aNew York, NY [u.a.]$$bElsevier$$c2014
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000171712 520__ $$aSodium iron fluorophosphate Na2FePO4F is a candidate positive electrode material for both lithium-ion batteries and sodium-ion batteries. We report the synthesis of Na2FePO4F/carbon powders by the simple and easily up-scalable technique of spray-drying. An aqueous solution containing citric acid as a carbon source was sprayed in a pilot-scale spray-dryer. Heat treatment at 600 °C in argon for 12 h was found appropriate to obtain single-phase Na2FePO4F; only 1.8% of Fe (III) was detected by iron-57 Mössbauer spectroscopy. When cycled against lithium, the discharge capacity reached 110 mA h/g at C/15 rate.
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000171712 7001_ $$0P:(DE-HGF)0$$aKrins, Natacha$$b1
000171712 7001_ $$0P:(DE-HGF)0$$aSchrijnemakers, Audrey$$b2
000171712 7001_ $$0P:(DE-HGF)0$$aCloots, Rudi$$b3
000171712 7001_ $$0P:(DE-HGF)0$$aVertruyen, Bénédicte$$b4
000171712 7001_ $$0P:(DE-HGF)0$$aBoschini, Frédéric$$b5$$eCorresponding Author
000171712 7001_ $$0P:(DE-Juel1)130706$$aHermann, Raphael$$b6
000171712 773__ $$0PERI:(DE-600)1491964-3$$a10.1016/j.matlet.2014.05.121$$gVol. 130, p. 263 - 266$$p263 - 266$$tMaterials letters$$v130$$x0167-577X$$y2014
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