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037 _ _ |a FZJ-2014-05397
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|a Gubanova, N. N.
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245 _ _ |a Structure of zirconium dioxide based porous glasses
260 _ _ |a Moscow
|b MAIK Nauka/Interperiodics Publ.
|c 2014
336 7 _ |a Journal Article
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520 _ _ |a This study is devoted to investigation of the micro- and mesostructure (including fractal properties) of porous zirconia glasses synthesized by precipitation from zirconium n-propoxide solutions in the presence of different hydrolyzing-agent (H2O) quantities at different temperatures. Analysis of small-angle neutron, ultra-small-angle neutron and X-ray scattering, scanning electron microscopy allows concluding that the synthesized glasses are complex systems with a three-level hierarchical fractal structure. It is revealed that both the temperature of synthesis and the H2O concentration in the initial solution significantly affect the structural characteristics of the glasses.
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