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@ARTICLE{Jaksch:171841,
      author       = {Jaksch, Sebastian and Schulz, Anita and Kyriakos,
                      Konstantinos and Zhang, Jianqi and Grillo, Isabelle and
                      Pipich, Vitaliy and Jordan, Rainer and Papadakis, Christine
                      M.},
      title        = {{T}he collapse and aggregation of thermoresponsive
                      poly(2-oxazoline) gradient copolymers: a time-resolved
                      {SANS} study},
      journal      = {Colloid $\&$ polymer science},
      volume       = {292},
      number       = {10},
      issn         = {0023-2904},
      address      = {Berlin},
      publisher    = {Springer},
      reportid     = {FZJ-2014-05398},
      pages        = {2413 - 2425},
      year         = {2014},
      abstract     = {We have investigated the collapse transition of aqueous
                      solutions of gradient copolymers from
                      poly(iso-propyl-2-oxazoline)s (PiPrOx), which contain few
                      hydrophobic moieties (n-nonyl-2-oxazoline (NOx) monomers).
                      We extend our previous investigations (Salzinger et al.,
                      Colloid Polym Sci 290:385–400, 2012), where, for the
                      gradient copolymers, an intermediate regime right above the
                      cloud point was identified where small aggregates are
                      predominant. Large aggregates are present in significant
                      numbers only at higher temperatures. To investigate the
                      stability of the intermediate regime, we performed
                      time-resolved small-angle neutron scattering (SANS)
                      experiments during temperature jumps starting below the
                      cloud point and ending in the intermediate regime or in the
                      high-temperature regime. We found that the intermediate
                      regime is stable during the time investigated (∼1 h).
                      Moreover, the collapse of the small aggregates and the
                      surface structure of the large aggregates are related to the
                      number of hydrophobic moieties and the quench depth. The
                      present results elucidate the structural evolution of these
                      polymers and relate them to their final state as well as to
                      their macroscopic behavior.},
      cin          = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
                      (München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
      ddc          = {540},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-1-20110106},
      pnm          = {54G - JCNS (POF2-54G24)},
      pid          = {G:(DE-HGF)POF2-54G24},
      experiment   = {EXP:(DE-MLZ)KWS3-20140101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000342172300002},
      doi          = {10.1007/s00396-014-3333-6},
      url          = {https://juser.fz-juelich.de/record/171841},
}