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@ARTICLE{Park:173018,
author = {Park, D. and Herpers, Anja and Menke, Tobias and
Heidelmann, Markus and Houben, Lothar and Dittmann, Regina
and Mayer, Joachim},
title = {{S}tudies of {L}ocal {S}tructural {D}isortions in
{S}trained {U}ltrathin {B}a{T}i{O}3 {F}ilms sing {S}canning
{T}ransmission {E}lectron {M}icroscopy},
journal = {Microscopy and microanalysis},
volume = {20},
issn = {1431-9276},
address = {New York, NY},
publisher = {Cambridge University Press},
reportid = {FZJ-2014-06431},
pages = {740 -747},
year = {2014},
abstract = {Ultrathin ferroelectric heterostructures
(SrTiO3/BaTiO3/BaRuO3/SrRuO3) were studied by scanning
transmission electron microscopy (STEM) in terms of
structural distortions and atomic displacements. The
TiO2-termination at the top interface of the BaTiO3 layer
was changed into a BaO-termination by adding an additional
BaRuO3 layer. High-angle annular dark-field (HAADF) imaging
by aberration-corrected STEM revealed that an artificially
introduced BaO-termination can be achieved by this interface
engineering. By using fast sequential imaging and
frame-by-frame drift correction, the effect of the specimen
drift was significantly reduced and the signal-to-noise
ratio of the HAADF images was improved. Thus, a quantitative
analysis of the HAADF images was feasible, and an in-plane
and out-of-plane lattice spacing of the BaTiO3 layer of 3.90
and 4.22 Å were determined. A 25 pm shift of the Ti columns
from the center of the unit cell of BaTiO3 along the c-axis
was observed. By spatially resolved electron energy-loss
spectroscopy studies, a reduction of the crystal field
splitting (CFS, ΔL3=1.93 eV) and an asymmetric broadening
of the e g peak were observed in the BaTiO3 film. These
results verify the presence of a ferroelectric polarization
in the ultrathin BaTiO3 film.},
cin = {PGI-5},
ddc = {570},
cid = {I:(DE-Juel1)PGI-5-20110106},
pnm = {424 - Exploratory materials and phenomena (POF2-424)},
pid = {G:(DE-HGF)POF2-424},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000339158700014},
doi = {10.1017/S1431927614000518},
url = {https://juser.fz-juelich.de/record/173018},
}