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@ARTICLE{Lewis:17344,
author = {Lewis, F.W. and Harwood, L.M. and Hudson, M.J. and Drew,
M.G.B. and Desreux, J.F. and Vidick, G. and Bouslimani, N.
and Modolo, G. and Wilden, A. and Sypula, M. and Vu, T.-H.
and Simonin, J.-P.},
title = {{H}ighly {E}fficient {S}eparation of {A}ctinides from
{L}anthanides by a {P}henantrholine-{D}erived
{B}is-{T}riazine {L}igand},
journal = {Journal of the American Chemical Society},
volume = {133},
issn = {0002-7863},
address = {Washington, DC},
publisher = {American Chemical Society},
reportid = {PreJuSER-17344},
pages = {13093 - 13102},
year = {2011},
note = {We thank the Nuclear Fission Safety Program of the European
Union for support under the ACSEPT (FP7-CP-2007-211 267)
contract. We also thank the EPSRC and the University of
Reading for funds for the X-Calibur system. Use of the
Chemical Analysis Facility at the University of Reading is
gratefully acknowledged.},
abstract = {The synthesis, lanthanide complexation, and solvent
extraction of actinide(III) and lanthanide(III) radiotracers
from nitric acid solutions by a phenanthroline-derived
quadridentate bis-triazine ligand are described. The ligand
separates Am(III) and Cm(III) from the lanthanides with
remarkably high efficiency, high selectivity, and fast
extraction kinetics compared to its 2,2'-bipyridine
counterpart. Structures of the 1:2 bis-complexes of the
ligand with Eu(III) and Yb(III) were elucidated by X-ray
crystallography and force field calculations, respectively.
The Eu(III) bis-complex is the first 1:2 bis-complex of a
quadridentate bis-triazine ligand to be characterized by
crystallography. The faster rates of extraction were
verified by kinetics measurements using the rotating
membrane cell technique in several diluents. The improved
kinetics of metal ion extraction are related to the higher
surface activity of the ligand at the phase interface. The
improvement in the ligand's properties on replacing the
bipyridine unit with a phenanthroline unit far exceeds what
was anticipated based on ligand design alone.},
keywords = {J (WoSType)},
cin = {IEK-6},
ddc = {540},
cid = {I:(DE-Juel1)IEK-6-20101013},
pnm = {Nukleare Sicherheitsforschung / ACSEPT - Actinide reCycling
by SEParation and Transmutation (211267)},
pid = {G:(DE-Juel1)FUEK404 / G:(EU-Grant)211267},
shelfmark = {Chemistry, Multidisciplinary},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:21770458},
UT = {WOS:000294591300039},
doi = {10.1021/ja203378m},
url = {https://juser.fz-juelich.de/record/17344},
}