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@ARTICLE{EndlerSchuck:18147,
author = {Endler-Schuck, C. and Leonide, A. and Weber, A. and
Uhlenbruck, S. and Tietz, F. and Ivers-Tiffée, E.},
title = {{P}erformance analysis of mixed ionic–electronic
conducting cathodes in anode supported cells},
journal = {Journal of power sources},
volume = {196},
issn = {0378-7753},
address = {New York, NY [u.a.]},
publisher = {Elsevier},
reportid = {PreJuSER-18147},
pages = {7257 - 7262},
year = {2011},
note = {Record converted from VDB: 12.11.2012},
abstract = {The analysis of mixed ionic electronic conducting (MIEC)
cathodes with respect to operation temperature and time is
essential for a target-oriented development of
anode-supported solid oxide fuel cells (ASCs). This study
tracks both issues by impedance spectroscopy on a
high-performance cathode with the composition
La0.58Sr0.4Co0.2Fe0.8O3-delta (LSCF).A wide set of impedance
spectra were sampled at 600,750 and 900 degrees C over the
entire operation time of 1000 h. The identification and
quantification of the individual anodic and cathodic
contributions to the polarization losses of an ASC were
enabled by an appropriate equivalent circuit model. For this
purpose, the impedance data sets were evaluated subsequently
by (i) a DRT (distribution of relaxation times) analysis
followed by (ii) a CNLS fit. The cathodic polarization
resistance is attributed to the oxygen surface exchange and
the bulk diffusion of oxygen ions and is described by a
Gerischer element.The anodic polarization resistance is
described by a Warburg element and two RQ elements according
to physical origins. The thorough analysis of all data sets
leads to the surprising outcome that the cathode degradation
is most pronounced and moreover, increases with decreasing
temperature. After 1000 h of operation, the cathode
polarization resistance raised steeply from $0.012\%/h$ at
900 degrees C over $0.28\%/h$ at 750 degrees C to $1.49\%/h$
at 600 degrees C. These latest findings will have
far-reaching implications for the development of MIEC
cathodes. (C) 2010 Elsevier B.V. All rights reserved.},
keywords = {J (WoSType)},
cin = {IEK-1},
ddc = {620},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {Rationelle Energieumwandlung},
pid = {G:(DE-Juel1)FUEK402},
shelfmark = {Electrochemistry / Energy $\&$ Fuels},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000292661800028},
doi = {10.1016/j.jpowsour.2010.11.079},
url = {https://juser.fz-juelich.de/record/18147},
}