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@ARTICLE{Wang:18219,
author = {Wang, W. and Dong, H. and Pacheco, V. and Willbold, D. and
Zhang, Y. and Offenhäusser, A. and Hartmann, R. and
Weirich, T. and Ma, P. and Krause, H. J. and Gu, Z.},
title = {{R}elaxation behavior study of ultra-small
superparamagnetic iron oxide nanoparticles at ultra-low and
ultra-high magnetic fields},
journal = {The journal of physical chemistry / B},
volume = {115},
issn = {1520-6106},
address = {Washington, DC},
publisher = {Soc.},
reportid = {PreJuSER-18219},
pages = {14789 - 14793},
year = {2011},
note = {We would like to thank F. Dorn for TEM imaging, J.
Bachhausen for IR measurements, and H. Lippert for the
ICP-OES measurements. This work is supported by the Research
Center Juelich, the China Scholarship Council (CSC), and the
German Helmholtz Association.},
abstract = {Ultrasmall superparamagnetic iron oxide nanoparticles
(USPIOs) have attracted attention because of their current
and potential usefulness as contrast agents for magnetic
resonance imaging (MRI) and nuclear magnetic resonance
(NMR). USPIOs are usually used for their significant
capacity to produce predominant proton relaxation effects,
which result in signal reduction. However, most previous
studies that utilized USPIOs have been focused on the
relaxation behavior at commonly used magnetic fields of
clinical MRI systems (typically 1-3 T). In this paper,
magnetic relaxation processes of protons in water
surrounding the USPIOs are studied at ultralow (≤10 mT)
and ultrahigh magnetic fields (14.1 T). USPIOs used in our
experiments were synthesized with a core size of 6 nm, and
transferred from organic to water by ligand exchange. The
proton spin-lattice relaxation time (T(1)) and spin-spin
relaxation time (T(2)) were investigated at ultralow (212
μT for T(2) and 10 mT for T(1)) and at 14.1 T with
different iron concentrations. At all of the fields, there
is a linear relationship between the inverse of relaxation
times and the iron concentration. The spin-spin relaxivity
(r(2)) at 14.1 T is much larger than that value of the
ultralow field. At ultralow field, however, the spin-lattice
relaxivity (r(1)) is larger than the r(1) at ultrahigh
field. The results provide a perspective on potential in
vivo and in vitro applications of USPIOs in ultralow and
ultrahigh field NMR and MRI.},
keywords = {Contrast Media: chemistry / Ferric Compounds: chemistry /
Magnetic Fields / Magnetite Nanoparticles: chemistry /
Solubility / Water: chemistry / Contrast Media (NLM
Chemicals) / Ferric Compounds (NLM Chemicals) / Magnetite
Nanoparticles (NLM Chemicals) / ferric oxide (NLM Chemicals)
/ Water (NLM Chemicals) / J (WoSType)},
cin = {ICS-6 / PGI-8 / ICS-8},
ddc = {530},
cid = {I:(DE-Juel1)ICS-6-20110106 / I:(DE-Juel1)PGI-8-20110106 /
I:(DE-Juel1)ICS-8-20110106},
pnm = {Funktion und Dysfunktion des Nervensystems / Grundlagen
für zukünftige Informationstechnologien / BioSoft:
Makromolekulare Systeme und biologische
Informationsverarbeitung},
pid = {G:(DE-Juel1)FUEK409 / G:(DE-Juel1)FUEK412 /
G:(DE-Juel1)FUEK505},
shelfmark = {Chemistry, Physical},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:21972868},
UT = {WOS:000297608600051},
doi = {10.1021/jp2066138},
url = {https://juser.fz-juelich.de/record/18219},
}