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@ARTICLE{Cattoz:185712,
author = {Cattoz, Beatrice and de Vos, Wiebe M. and Cosgrove, Terence
and Crossman, Martin and Appavou, Marie-Sousai and Prescott,
Stuart W.},
title = {{C}omplexation of polymeric stabilisers in solution and at
the silica nanoparticle interface},
journal = {Colloids and surfaces / A},
volume = {449},
issn = {0927-7757},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2014-07137},
pages = {57 - 64},
year = {2014},
abstract = {The weak polyelectrolyte sodium polyacrylate, NaPA, and the
neutral poly(vinyl pyrrolidone), PVP, were combined and the
effects of complexation both in solution and at the
nanoparticle interface were studied under basic pH
conditions. Using a combination of SANS and PCS, we
demonstrate that attractive inter-polymer interactions occur
between PVP and NaPA in solution (for polymers with
molecular weights equal to 40 K and 60 K respectively);
typically, no attractive interactions between PVP and NaPA
are reported above a critical pH of 4–5. Polymer
interactions in the bulk are observed between the larger
molecular weight polymers studied. The mass ratios of
polymer also affect the interactions in the bulk, indicating
that polymer interactions are influenced by the charges
present in the system. The addition of NaPA to a silica
dispersion with PVP previously adsorbed to the particles is
shown to led to polymer desorption and the destabilisation
of the system leading to particle aggregation or even
flocculation. SANS data show that the interparticle
potential changes from being repulsive with bare silica or
PVP-coated silica to attractive on addition of NaPA. The
molecular weight of PVP is seen to affect the amount of
polymer desorbed, whereas the molecular weight of NaPA had
an effect on the aggregation of particles.},
cin = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
(München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1 /
ICS-1},
ddc = {540},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-1-20110106 / I:(DE-Juel1)ICS-1-20110106},
pnm = {54G - JCNS (POF2-54G24)},
pid = {G:(DE-HGF)POF2-54G24},
experiment = {EXP:(DE-MLZ)KWS1-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000335202400007},
doi = {10.1016/j.colsurfa.2014.02.039},
url = {https://juser.fz-juelich.de/record/185712},
}