000186435 001__ 186435 000186435 005__ 20240619092039.0 000186435 0247_ $$2doi$$a10.1021/ma502056y 000186435 0247_ $$2ISSN$$a0024-9297 000186435 0247_ $$2ISSN$$a1520-5835 000186435 0247_ $$2WOS$$aWOS:000347138300026 000186435 037__ $$aFZJ-2015-00511 000186435 082__ $$a540 000186435 1001_ $$0P:(DE-HGF)0$$aDubbert, Janine$$b0 000186435 245__ $$aHow Hollow Are Thermoresponsive Hollow Nanogels? 000186435 260__ $$aWashington, DC$$bSoc.$$c2014 000186435 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article$$bjournal$$mjournal$$s1421333861_12761 000186435 3367_ $$2DataCite$$aOutput Types/Journal article 000186435 3367_ $$00$$2EndNote$$aJournal Article 000186435 3367_ $$2BibTeX$$aARTICLE 000186435 3367_ $$2ORCID$$aJOURNAL_ARTICLE 000186435 3367_ $$2DRIVER$$aarticle 000186435 520__ $$aA main challenge in colloid science is the development of smart delivery systems that store and protect actives from degradation and allow release in response to an external stimulus like temperature. Hollow nanogel capsules made of temperature-sensitive polymers are particularly promising materials. The stimuli-sensitive void size, shell thickness, and permeability determine cargo storage and its release behavior. Thus, determination and control of these morphological parameters are of outmost relevance for the design of new, functional drug delivery vehicles. Here we investigate quantitatively void size and shell thickness of hollow nanogels at different states of swelling by means of small-angle neutron scattering (SANS) employing contrast variation. We demonstrate the structure-sensitivity dilemma: hollow nanogels with a slightly cross-linked shell reveal distinct temperature sensitivity but possess nearly no void (14% of the initial core volume) and are thus hardly “hollow”. 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