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000186443 0247_ $$2doi$$a10.1007/s00396-013-2923-z
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000186443 1001_ $$0P:(DE-HGF)0$$aKim, Chang J.$$b0$$eCorresponding Author
000186443 245__ $$aSynthesis and characterization of polystyrene chains on the surface of silica nanoparticles: comparison of SANS, SAXS, and DLS results
000186443 260__ $$aBerlin$$bSpringer$$c2013
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000186443 520__ $$aAn extensive characterization of well-defined polystyrene (PS)-grafted silica nanoparticles is reported. Bare SiO2 particles (diameter 50 nm) were functionalized with a suitable initiator for the surface-initiated anionic polymerization of styrene. Both grafted and free PS chains were characterized and compared by size-exclusion chromatography (SEC). PS-grafted particles were characterized by transmission electron microscopy (TEM), thermogravimetric analysis (TGA), small-angle x-ray scattering (SAXS), small-angle neutron scattering (SANS), and dynamic light scattering (DLS). The thickness of the grafted PS chains was obtained by SANS and DLS and scaled with M0.6w displaying similar behavior with free PS chains in the same solvent used, tetrahydrofuran (THF). Grafting densities obtained from SANS data and TGA were found to be small, and the thickness of the grafted PS chains determined by SANS was found to be similar to 2Rg of free PS chains in THF. Both results are consistent with a “coil-like” conformation of the grafted PS chains.
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000186443 65017 $$0V:(DE-MLZ)GC-1602-2016$$2V:(DE-HGF)$$aPolymers, Soft Nano Particles and  Proteins$$x2
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000186443 65017 $$0V:(DE-MLZ)GC-140$$2V:(DE-HGF)$$aSoft Matter, Macromolecules, Complex fluids, Biophysics$$x0
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000186443 7001_ $$0P:(DE-HGF)0$$aSondergeld, Katrin$$b1
000186443 7001_ $$0P:(DE-HGF)0$$aMazurowski, Markus$$b2
000186443 7001_ $$0P:(DE-HGF)0$$aGallei, Markus$$b3
000186443 7001_ $$0P:(DE-HGF)0$$aRehahn, Matthias$$b4
000186443 7001_ $$0P:(DE-HGF)0$$aSpehr, Tinka$$b5
000186443 7001_ $$0P:(DE-Juel1)130646$$aFrielinghaus, Henrich$$b6$$ufzj
000186443 7001_ $$0P:(DE-HGF)0$$aStühn, Bernd$$b7
000186443 773__ $$0PERI:(DE-600)1462029-7$$a10.1007/s00396-013-2923-z$$gVol. 291, no. 9, p. 2087 - 2099$$n9$$p2087 - 2099$$tColloid & polymer science$$v291$$x1435-1536$$y2013
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