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@ARTICLE{Kim:186443,
      author       = {Kim, Chang J. and Sondergeld, Katrin and Mazurowski, Markus
                      and Gallei, Markus and Rehahn, Matthias and Spehr, Tinka and
                      Frielinghaus, Henrich and Stühn, Bernd},
      title        = {{S}ynthesis and characterization of polystyrene chains on
                      the surface of silica nanoparticles: comparison of {SANS},
                      {SAXS}, and {DLS} results},
      journal      = {Colloid $\&$ polymer science},
      volume       = {291},
      number       = {9},
      issn         = {1435-1536},
      address      = {Berlin},
      publisher    = {Springer},
      reportid     = {FZJ-2015-00518},
      pages        = {2087 - 2099},
      year         = {2013},
      abstract     = {An extensive characterization of well-defined polystyrene
                      (PS)-grafted silica nanoparticles is reported. Bare SiO2
                      particles (diameter 50 nm) were functionalized with a
                      suitable initiator for the surface-initiated anionic
                      polymerization of styrene. Both grafted and free PS chains
                      were characterized and compared by size-exclusion
                      chromatography (SEC). PS-grafted particles were
                      characterized by transmission electron microscopy (TEM),
                      thermogravimetric analysis (TGA), small-angle x-ray
                      scattering (SAXS), small-angle neutron scattering (SANS),
                      and dynamic light scattering (DLS). The thickness of the
                      grafted PS chains was obtained by SANS and DLS and scaled
                      with M0.6w displaying similar behavior with free PS chains
                      in the same solvent used, tetrahydrofuran (THF). Grafting
                      densities obtained from SANS data and TGA were found to be
                      small, and the thickness of the grafted PS chains determined
                      by SANS was found to be similar to 2Rg of free PS chains in
                      THF. Both results are consistent with a “coil-like”
                      conformation of the grafted PS chains.},
      cin          = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
                      (München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1 /
                      ICS-1},
      ddc          = {540},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-1-20110106 / I:(DE-Juel1)ICS-1-20110106},
      pnm          = {451 - Soft Matter Composites (POF2-451) / 54G - JCNS
                      (POF2-54G24)},
      pid          = {G:(DE-HGF)POF2-451 / G:(DE-HGF)POF2-54G24},
      experiment   = {EXP:(DE-MLZ)KWS2-20140101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000323248000006},
      doi          = {10.1007/s00396-013-2923-z},
      url          = {https://juser.fz-juelich.de/record/186443},
}