Home > Publications database > Polystyrene Brushes on Fully Deuterated Organic Nanoparticles by Surface-Initiated Nitroxide-Mediated Radical Polymerization > print

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024 7 _ |2 doi
|a 10.1002/macp.201200733
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|a Mazurowski, Markus
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245 _ _ |a Polystyrene Brushes on Fully Deuterated Organic Nanoparticles by Surface-Initiated Nitroxide-Mediated Radical Polymerization
260 _ _ |a Weinheim
|b Wiley-VCH
|c 2013
336 7 _ |a Journal Article
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520 _ _ |a The synthesis of polystyrene (PS) brushes on fully deuterated PS nanoparticles by surface-initiated nitroxide-mediated radical polymerization (SI-NMRP) is reported. Due to the high demand of deuterated monomers, an efficient deuteration procedure of suitable and readily available precursors is developed. SI-NMRP of styrene is improved regarding reaction control, grafting density, and conversion. Insights into the scaling behavior and conformational features of surface-attached PS chains on deuterated particles are investigated by using dynamic light scattering measurements, proving that polymer brushes are formed. The particles with surface-attached initiator are shown to be uniform spherical core-shell particles by small-angle neutron scattering measurements.
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|t Macromolecular chemistry and physics
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