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@INPROCEEDINGS{Reppert:188042,
author = {Reppert, Thorsten and Tsai, Chih-Long and Finsterbusch,
Martin and Uhlenbruck, Sven and Guillon, Olivier and Bram,
Martin},
title = {{O}xide-ceramic electrolyte layers for all-solid-state
lithium batteries},
reportid = {FZJ-2015-01520},
year = {2015},
abstract = {In the past decade, electricity generated from renewable
energy sources, as well as electro mobility have gained much
importance in our society. With this readiness to change the
current system, an increase of requirements for electric
grid and safety aspects of energy storage systems appear.
All-solid-state lithium batteries (ASB) have better safety
properties due to the non-flammable solid electrolyte than
common lithium ion batteries (LIB), which use flammable
organic liquid as electrolyte. Additionally, a higher energy
density is possible because of their compatibility with
using high voltage cathode materials. Oxide-ceramic lithium
ion conductors such as Li7La3Zr2O12 (LLZ) [1] have the
advantage of inertness in oxygen atmosphere, which
simplifies their handling during the material processing.
LLZ’s stability when contacting lithium metal and its wide
electrochemical window (usable up to 8V vs. Li/Li+) would
provide higher energy densities than LIB. In combination
with its good total ion conductivity of about 10-4 S cm-1 at
room temperature [2], it is one of the most promising
candidates for all-solid-state battery application. LLZ was
synthesized and by substitution of Al [2], Ta [3] and Y [4]
into the LLZ structure, the structural stability and its
total ion conductivity were improved. Ta substituted LLZ
indicated a highest total ion conductivity of about 10-3 S
cm-1 and almost no dependence on its lithium concentration.
After investigation of bulk electrolyte materials, an ASB
prototype cell using bulk LLZ as solid electrolyte was
fabricated at IEK-1 and proved to run a LED. To bridge lab
works and real applications, large size LLZ functional
layers need to be fabricated by different established
technologies. Therefore, the investigated LLZ has been
processed by tape casting and was used for sintering
studies, in order to obtain highly dense solid electrolyte
layers and also mixed electrode films for prospective
all-solid-state lithium battery application.References:[1]
Murugan et al., Angew. Chem. Int. Ed. 46 (2007) 7778.[2]
Hubaud et al., J. Mater. Chem. A. 1 (2013) 8813. [3]
Buschmann et al., Phys. Chem. Chem. Phys. 13 (2011)
19378.[4] Murugan et. al., Electrochem. Commun. 13 (2011)
1373.},
month = {Jan},
date = {2015-01-21},
organization = {Batterieforum Deutschland 2015, Berlin
(Germany), 21 Jan 2015 - 23 Jan 2015},
cin = {IEK-1 / JARA-ENERGY},
cid = {I:(DE-Juel1)IEK-1-20101013 / $I:(DE-82)080011_20140620$},
pnm = {131 - Electrochemical Storage (POF3-131) / HITEC -
Helmholtz Interdisciplinary Doctoral Training in Energy and
Climate Research (HITEC) (HITEC-20170406)},
pid = {G:(DE-HGF)POF3-131 / G:(DE-Juel1)HITEC-20170406},
typ = {PUB:(DE-HGF)24},
url = {https://juser.fz-juelich.de/record/188042},
}