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@ARTICLE{MacLaren:189240,
author = {MacLaren, Ian and Wang, LiQiu and McGrouther, Damien and
Craven, Alan J. and McVitie, Stephen and Schierholz, Roland
and Kovács, András and Barthel, Juri and Dunin-Borkowski,
Rafal},
title = {{O}n the origin of differential phase contrast at a locally
charged and globally charge-compensated domain boundary in a
polar-ordered material},
journal = {Ultramicroscopy},
volume = {154},
issn = {0304-3991},
address = {Amsterdam},
publisher = {Elsevier Science},
reportid = {FZJ-2015-02428},
pages = {57 - 63},
year = {2015},
abstract = {Differential phase contrast (DPC) imaging in the scanning
transmission electron microscope is applied to the study of
a charged antiphase domain boundary in doped bismuth
ferrite. A clear differential signal is seen, which matches
the expected direction of the electric field at the
boundary. However, further study by scanned diffraction
reveals that there is no measurable deflection of the
primary diffraction disc and hence no significant free
E-field in the material. Instead, the DPC signal arises from
a modulation of the intensity profile within the primary
diffraction disc in the vicinity of the boundary.
Simulations are used to show that this modulation arises
purely from the local change in crystallographic structure
at the boundary and not from an electric field. This study
highlights the care that is required when interpreting
signals recorded from ferroelectric materials using both DPC
imaging and other phase contrast techniques.},
cin = {PGI-5 / IEK-9},
ddc = {570},
cid = {I:(DE-Juel1)PGI-5-20110106 / I:(DE-Juel1)IEK-9-20110218},
pnm = {143 - Controlling Configuration-Based Phenomena (POF3-143)},
pid = {G:(DE-HGF)POF3-143},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000355018700009},
doi = {10.1016/j.ultramic.2015.03.016},
url = {https://juser.fz-juelich.de/record/189240},
}