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000189246 0247_ $$2doi$$a10.1016/j.solidstatesciences.2014.11.002
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000189246 1001_ $$0P:(DE-HGF)0$$aGrzechnik, Andrzej$$b0$$eCorresponding Author
000189246 245__ $$aCrystal structure and high-pressure stability of hydrothermally grown LiKTmF$_{5}$
000189246 260__ $$aAmsterdam [u.a.]$$bElsevier$$c2015
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000189246 520__ $$aSingle crystals of LiKTmF5 were grown hydrothermally. Its crystal structure was studied with single-crystal X-ray diffraction to 8.6 GPa. The material is monoclinic (P21/c, Z = 4) and does not undergo any phase transition in the pressure range studied here. The analysis of its pseudosymmetry with respect to the minimal k-supergroup C2/m reveals that the deviations of the individual atoms from the respective higher symmetrical positions in C2/m are increasing on compression, i.e., due to the reduction of the unit-cell volume. Such a behaviour is the opposite of the effect of incorporation of various M cations in the LiKMF5 materials (M:Y and rare earths) at atmospheric conditions, since LiKYbF5 and LiKLuF5 with the smallest unit cells crystallize in space group C2/m, while LiLYF5 with a larger unit cell has P21/c symmetry.
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000189246 7001_ $$0P:(DE-HGF)0$$aComer, Sara$$b1
000189246 7001_ $$0P:(DE-HGF)0$$aKolis, Joseph W.$$b2
000189246 7001_ $$0P:(DE-Juel1)145694$$aFriese, Karen$$b3
000189246 773__ $$0PERI:(DE-600)2035101-X$$a10.1016/j.solidstatesciences.2014.11.002$$gVol. 39, p. 40 - 44$$p40 - 44$$tSolid state sciences$$v39$$x1293-2558$$y2015
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