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@ARTICLE{Kusmin:18981,
author = {Kusmin, A. and Lechner, R.E. and Saenger, W.},
title = {{Q}uasielastic small-angle neutron scattering from heavy
water solutions of cyclodextrins},
journal = {The journal of chemical physics},
volume = {134},
issn = {0021-9606},
address = {Melville, NY},
publisher = {American Institute of Physics},
reportid = {PreJuSER-18981},
pages = {024518},
year = {2011},
note = {R.E.L. thanks G. Steiner and B. Urban for very valuable
technical assistance during the NEAT experiment. Two of us
(A.K. and RE.L.) thank the Hahn-Meitner-Institut for its
hospitality. Financial support for A.K. by the Institute of
Chemistry and Biochemistry of the Freie Universitat Berlin
is gratefully acknowledged.},
abstract = {We present a model for quasielastic neutron scattering
(QENS) by an aqueous solution of compact and inflexible
molecules. This model accounts for time-dependent spatial
pair correlations between the atoms of the same as well as
of distinct molecules and includes all coherent and
incoherent neutron scattering contributions. The extension
of the static theory of the excluded volume effect [A. K.
Soper, J. Phys.: Condens. Matter 9, 2399 (1997)] to the
time-dependent (dynamic) case allows us to obtain simplified
model expressions for QENS spectra in the low Q region in
the uniform fluid approximation. The resulting expressions
describe the quasielastic small-angle neutron scattering
(QESANS) spectra of D(2)O solutions of native and methylated
cyclodextrins well, yielding in particular translational and
rotational diffusion coefficients of these compounds in
aqueous solution. Finally, we discuss the full potential of
the QESANS analysis (that is, beyond the uniform fluid
approximation), in particular, the information on
solute-solvent interactions (e.g., hydration shell
properties) that such an analysis can provide, in
principle.},
keywords = {Cyclodextrins: chemistry / Deuterium Oxide: chemistry /
Diffusion / Rotation / Scattering, Small Angle / Solutions /
X-Ray Diffraction / Cyclodextrins (NLM Chemicals) /
Solutions (NLM Chemicals) / Deuterium Oxide (NLM Chemicals)
/ J (WoSType)},
cin = {ICS-1 / JCNS-1},
ddc = {540},
cid = {I:(DE-Juel1)ICS-1-20110106 / I:(DE-Juel1)JCNS-1-20110106},
pnm = {BioSoft: Makromolekulare Systeme und biologische
Informationsverarbeitung / Großgeräte für die Forschung
mit Photonen, Neutronen und Ionen (PNI)},
pid = {G:(DE-Juel1)FUEK505 / G:(DE-Juel1)FUEK415},
shelfmark = {Physics, Atomic, Molecular $\&$ Chemical},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:21241131},
UT = {WOS:000286471900059},
doi = {10.1063/1.3518367},
url = {https://juser.fz-juelich.de/record/18981},
}