%0 Conference Paper
%A Almeida, T. P.
%A Muxworhty
%A Williams, W.
%A Kasama, T.
%A Dunin-Borkowski, Rafal
%T Hydrothermal synthesis, off-axis electron holography and magnetic properties of Fe$_{3}$O$_{4}$ nanoparticles
%J Journal of physics / Conference Series
%V 522
%N 1
%@ 1742-6588
%C Bristol
%I IOP Publ.
%M FZJ-2015-02907
%P 012062
%D 2014
%X The hydrothermal synthesis of Fe3O4 nanoparticles (NPs) (< 50 nm) from mixed FeCl3 / FeCl2 precursor solution at pH ~ 12 has been confirmed using complementary characterisation techniques of transmission electron microscopy and X-ray diffractometry. Off-axis electron holography allowed for visualisation of their single domain (SD) nature, as well as inter-particle interactions, with the latter attributed to explain the pseudo-SD/multi-domain behaviour demonstrated by bulk magnetic measurements.
%B Paper presented at EMAG 2013
%C 3 Sep 2014 - 6 Sep 2014, York (United Kingdom)
Y2 3 Sep 2014 - 6 Sep 2014
M2 York, United Kingdom
%F PUB:(DE-HGF)8 ; PUB:(DE-HGF)16
%9 Contribution to a conference proceedingsJournal Article
%U <Go to ISI:>//WOS:000340969200062
%R 10.1088/1742-6596/522/1/012062
%U https://juser.fz-juelich.de/record/189938