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@INPROCEEDINGS{Tsai:189990,
author = {Tsai, Chih-Long and Dellen, Christian and Reppert, Thorsten
and Uhlenbruck, Sven and Buchkremer, Hans Peter and Guillon,
Olivier},
title = {{A}ll solid state {L}i battery using garnet structure
{T}a-substituted {L}i7{L}a3{Z}r2{O}12 as solid electrolyte},
reportid = {FZJ-2015-02953},
year = {2015},
abstract = {All solid state Li battery containing oxide-class solid
electrolyte is considered to be out stand from their high
safety and higher energy density. Compared to the other
class the solid Li ionic conductors, oxide-class Li ion
conductors have additional advantages of easier material
handling during synthesis, higher chemical stability and
wider electrochemical window[1-4].In order to realize the
using of oxide-class Li ion conductor as solid electrolyte
for a Li battery, Ta-substituted Li7La3Zr2O12 (LLZ:Ta)
powder had been synthesized via solid state reaction. LLZ:Ta
with an optimized sintering parameter exhibits a high Li ion
conductivity of 7.8 x 10-4 S cm-1 at 30 oC with a relative
density of $~94\%.$ By hot pressing, the relative density of
LLZ:Ta was increased to > $99\%$ with an Li ion conductivity
of 1.18 x10-3 S cm-1. The material was further implanted as
a solid electrolyte by using screen printing to put on
LiCoO2 as cathode. Afterward, a metallic Li foil was used as
anode by mechanical press onto the pellet. The built Li
battery with LLZ:Ta exhibited good charge-discharge
utilization of active material up to $80\%$ which equal to a
capacity density of ~580 Ah cm-2 at 100 oC. It also
exhibited good cycle ability that hundreds of cycle were
achieved at temperature of 45 oC. Thus, LLZ:Ta shows as a
promising candidate for all solid state Li battery. However,
the reduction of high internal resistance of the cell is
still maintained as the major challenge to further
improvement of the battery performance, especially if the
application of this all solid state Li battery is toward
room temperature. During this presentation, the material
properties of LLZ:Ta, the test results which include
microstructure and electrochemical performances from Li
battery by using LLZ:Ta and the challenges of building up Li
battery by using LLZ:Ta will be discussed.},
month = {Apr},
date = {2015-04-27},
organization = {Batterietag/Kraftwerk Batterie 2015,
Aachen (Germany), 27 Apr 2015 - 29 Apr
2015},
subtyp = {After Call},
cin = {IEK-1},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {131 - Electrochemical Storage (POF3-131) / HITEC -
Helmholtz Interdisciplinary Doctoral Training in Energy and
Climate Research (HITEC) (HITEC-20170406)},
pid = {G:(DE-HGF)POF3-131 / G:(DE-Juel1)HITEC-20170406},
typ = {PUB:(DE-HGF)6},
url = {https://juser.fz-juelich.de/record/189990},
}