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000019093 084__ $$2WoS$$aChemistry, Physical
000019093 084__ $$2WoS$$aMaterials Science, Multidisciplinary
000019093 084__ $$2WoS$$aPhysics, Multidisciplinary
000019093 084__ $$2WoS$$aPolymer Science
000019093 1001_ $$0P:(DE-HGF)0$$aSen, D.$$b0
000019093 245__ $$aArrest of morphological transformation during evaporation-induced self-assembly of mixed colloids in micrometric droplets by charge tuning
000019093 260__ $$aCambridge$$bRoyal Society of Chemistry (RSC)$$c2011
000019093 300__ $$a5423 - 5429
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000019093 440_0 $$016881$$aSoft Matter$$v7$$x1744-683X$$y11
000019093 500__ $$aAuthors thank Dr S. Ramanathan of MSD, BARC for his kind help in zeta-potential measurements. DS would like to thank Drs Antoine Thill and Olivier Spalla of LIONS, SCM, DRECAM, CEA Saclay, France for many fruitful discussions on spray drying during his visit at CEA Saclay, France. DS and JB thankfully acknowledge financial support (DST(5)/AKR/P087/10-11/673) received from Department of Science and Technology, India through S. N. Bose National Centre for Basic Science, Kolkata, India for neutron scattering work at JCNS, Germany and ILL, France.
000019093 520__ $$aSelf-assembled grains of mixed colloids have been synthesized using evaporation induced self-assembly (EISA) by spray drying. We demonstrate using electron microscopy and small-angle neutron scattering experiments that buckling driven sphere to deformed-doughnut like morphological transformation in such a process can be arrested by proper tuning of the surface charge on the colloidal components. The buckling amplitude diminishes with a reduction in stabilization force between the colloidal particles. It is established that such arrest of morphological transformation is related to an effective exposure of the surface of softer component at gas-liquid interface. Scattering experiments confirm relatively more compact structure of the non-buckled grains compared to that of the buckled grains. A plausible mechanism regarding the arrest of morphological transformation by surface charge tuning is illustrated.
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000019093 7001_ $$0P:(DE-HGF)0$$aSavio Melo, J:$$b1
000019093 7001_ $$0P:(DE-Juel1)VDB103663$$aBahadur, J.$$b2$$uFZJ
000019093 7001_ $$0P:(DE-HGF)0$$aMazumder, S.$$b3
000019093 7001_ $$0P:(DE-HGF)0$$aBhattacharya, S.$$b4
000019093 7001_ $$0P:(DE-HGF)0$$aD'Souza, S.F.$$b5
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000019093 8567_ $$uhttp://dx.doi.org/10.1039/C1SM05100H
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