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@PHDTHESIS{Babajani:200870,
author = {Babajani, Ninet},
title = {{L}adungstransportuntersuchungen an nanofunktionalen
{B}auelementen mit {D}iodencharakteristik basierend auf
funktionalisierten {N}anopartikeln},
volume = {42},
school = {RWTH Aachen},
type = {Dr.},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2015-03241},
isbn = {978-3-95806-026-5},
series = {Schriften des Forschungszentrums Jülich. Reihe Information
/ information},
pages = {iv, 138, XLVII S.},
year = {2015},
note = {RWTH Aachen, Diss., 2014},
abstract = {The success of silicon-based information technology is
mainly based on its cost effectiveness and on its efficient
information storage in semiconductor memory cells. The
miniaturization of electronic components is a key element in
semiconductor technology that drives operating speed and
energy efficiency. However, further shrinking of device
structures will face huge technological challenges, so that
alternative technologies have to be considered. So called
hybrid concepts combine the existing silicon-based
electronics with new technologies such as molecular
electronics in which molecules or functionalized
nanoparticles are studied as electronic components. In this
work, different
electrode-molecule/nanoparticle/molecule-electrode devices
were investigated for their suitability as a diode device in
a CMOS compatible system. These arrangements were
systematically varied and the transport properties of
different mono- or bifunctionalized gold nanoparticles
(AuNPs) were characterized between homo- or heterometallic
nanoelectrodes (HoNE or HeNe). Mixed functionalized AuNPs
and Janus AuNPs (d = 14 $\pm$ 1 nm), with different
molecules on opposite hemispheres, were used as
bifunctionalized AuNP. The first step for understanding the
electron transport through these
electrode-molecule/AuNP/molecule-electrode devices was the
optimization and characterization of the individual
components of the devices. Investigations of the AuNPs and
AuNP adsorption on the different metals showed that the
binding of single-Janus-AuNPs can be controlled by the pH
buffer solution. Furthermore, surface-sensitive methods
(XPS) confirmed the functionality of the molecules after the
immobilization and drying and demonstrated the directed
orientation of the Janus-AuNPs. Optimizations in the process
of fabrication of HeNE, which involves electron-beam
lithography in combination with a hard mask, allowed to
produce HeNE, with a distance of d = 13 $\pm$ 2 nm, and a
yield of about 50\%. The AuNPs were immobilized between the
nano-electrodes by dielectrophoretic trapping. The
electrical characterization of the devices included the
analysis of the transport mechanisms, such as Arrhenius,
superexchange or tunneling transport. The tunnelling
transport was additionally analyzed by the Simmonsmodel,
Landauer formula and by „Transition Voltage
Spectroscopy“. The charge transport studies of mixed
functionalized AuNPs between the HeNe showed diode
characteristic due to the different HOMO/LUMO energies of
the twomolecules. However, mixed AuNPs showed an
uncontrolled orientation between the nanoelectrodes and
thus, random asymmetrical contacts are expected.
Alsomonofunctionalized AuNP were immobilized in order to
obtain diode characteristics. In this case the resulting
asymmetric contacts between the different metals and the
ligands should cause a rectifying behavior. However, the
diode characteristics remained unobserved due to water
molecules adsorbed to the ligand shell, which have an
approximately equal binding energy at both metal -molecule
contacts. Whereas for Janus AuNPs the targeted, directed
asymmetric I/U-characteristic can be proved due to the
different transmission coefficients of both
molecule-metal-contacts and the significantly different
HOMO/LUMO levels of themolecules on both hemispheres. In
addition to the tunneling process for the Janus-AuNP
devices, thermally activated transport processes were
observed under heliumor vacuum atmosphere.},
keywords = {Dissertation (GND)},
cin = {PGI-7},
cid = {I:(DE-Juel1)PGI-7-20110106},
pnm = {524 - Controlling Collective States (POF3-524)},
pid = {G:(DE-HGF)POF3-524},
typ = {PUB:(DE-HGF)11 / PUB:(DE-HGF)3},
url = {https://juser.fz-juelich.de/record/200870},
}