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@ARTICLE{Salzinger:201063,
      author       = {Salzinger, Stephan and Huber, Stephan and Jaksch, Sebastian
                      and Busch, Peter and Jordan, Rainer and Papadakis, Christine
                      M.},
      title        = {{A}ggregation behavior of thermo-responsive
                      poly(2-oxazoline)s at the cloud point investigated by {FCS}
                      and {SANS}},
      journal      = {Colloid $\&$ polymer science},
      volume       = {290},
      number       = {5},
      issn         = {1435-1536},
      address      = {Berlin},
      publisher    = {Springer},
      reportid     = {FZJ-2015-03373},
      pages        = {385 - 400},
      year         = {2012},
      abstract     = {We have studied different thermo-responsive
                      poly(2-oxazoline)s with iso-propyl (iPrOx) and n-propyl
                      (nPrOx) pendant groups in aqueous solutions, where they
                      exhibit lower critical solution temperature behavior. This
                      paper focuses on the effect of the degree of polymerization,
                      n, the concentration, c, in the dilute regime, and the
                      presence of hydrophobic moieties. The cloud points were
                      investigated as a function of the degree of polymerization,
                      n, and of the polymer concentration, c. The aggregation
                      behavior near the cloud point was studied by
                      temperature-resolved small-angle neutron scattering and
                      fluorescence correlation spectroscopy, i.e., a combination
                      of ensemble and single molecule methods. We found that at
                      the cloud points, large aggregates are formed and that the
                      cloud points depend strongly on both, n and c. Diblock
                      copolymers from iPrOx and nPrOx form large aggregates
                      already at the cloud point of PnPrOx, and, unexpectedly, no
                      micelles are observed between the cloud points of the two
                      blocks. Gradient copolymers from iPrOx and
                      n-nonyl-2-oxazoline (NOx) display a complex aggregation
                      behavior resulting from the interplay between intra- and
                      intermolecular association mediated by the hydrophobic NOx
                      blocks. Above the cloud point, an intermediate temperature
                      regime with a width of a few Kelvin was found with small but
                      stable polymer aggregates. Only at higher temperatures,
                      larger aggregates are found in significant number.},
      cin          = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
                      (München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
      ddc          = {540},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-1-20110106},
      pnm          = {54G - JCNS (POF2-54G24)},
      pid          = {G:(DE-HGF)POF2-54G24},
      experiment   = {EXP:(DE-MLZ)KWS1-20140101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000303510500001},
      doi          = {10.1007/s00396-011-2564-z},
      url          = {https://juser.fz-juelich.de/record/201063},
}