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@ARTICLE{Joos:201166,
      author       = {Joos, Jochen and Ender, Moses and Rotscholl, Ingo and
                      Menzler, Norbert H. and Ivers-Tiffée, Ellen},
      title        = {{Q}uantification of double-layer {N}i/{YSZ} fuel cell
                      anodes from focused ion beam tomography data},
      journal      = {Journal of power sources},
      volume       = {246},
      issn         = {0378-7753},
      address      = {New York, NY [u.a.]},
      publisher    = {Elsevier},
      reportid     = {FZJ-2015-03471},
      pages        = {819 - 830},
      year         = {2014},
      abstract     = {Three-dimensional microstructure reconstructions of
                      Ni–yttria-stabilized zirconia (Ni/YSZ) anodes are
                      presented, all of which are based on focused ion beam
                      tomography data.The reconstruction procedure, starting from
                      a series of 2D scanning electron micrographs, is
                      investigated step by step and potential sources of error are
                      identified. The distinction between Ni phase, YSZ phase and
                      pore phase is solved by an advanced algorithm, which belongs
                      to the region-growing image segmentation methods. This
                      improves the accuracy of automated grayscale segmentation
                      especially for images with low contrast, which is
                      characteristic of both solid phases in Ni/YSZ
                      anodes.Critical microstructure parameters like material
                      fractions, surface areas, particle size and distribution of
                      Ni, YSZ, and pore phase, as well as phase connectivity and
                      triple-phase boundary density, are evaluated and
                      discussed.In this contribution, two types of
                      high-performance Ni/YSZ anodes – differing in thickness of
                      both the anode functional layer and the anode substrate –
                      are reconstructed and compared to each other. For the first
                      time, the anode functional layer adjacent to the thin film
                      electrolyte is separately quantified. The presented methods
                      are qualified to quantitatively compare different anode
                      microstructures and relate the result to their
                      electrochemical performance.},
      cin          = {IEK-1},
      ddc          = {620},
      cid          = {I:(DE-Juel1)IEK-1-20101013},
      pnm          = {123 - Fuel Cells (POF2-123) / SOFC - Solid Oxide Fuel Cell
                      (SOFC-20140602)},
      pid          = {G:(DE-HGF)POF2-123 / G:(DE-Juel1)SOFC-20140602},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000326661100102},
      doi          = {10.1016/j.jpowsour.2013.08.021},
      url          = {https://juser.fz-juelich.de/record/201166},
}