TY - JOUR AU - Arcella, Annalisa AU - Dreyer, Jens AU - Ippoliti, Emiliano AU - Ivani, Ivan AU - Portella, Guillem AU - Gabelica, Valérie AU - Carloni, Paolo AU - Orozco, Modesto TI - Structure and Dynamics of Oligonucleotides in the Gas Phase JO - Angewandte Chemie / International edition VL - 54 IS - 2 SN - 1433-7851 CY - Weinheim PB - Wiley-VCH M1 - FZJ-2015-03628 SP - 467–471 PY - 2015 AB - By combining ion-mobility mass spectrometry experiments with sub-millisecond classical and ab initio molecular dynamics we fully characterized, for the first time, the dynamic ensemble of a model nucleic acid in the gas phase under electrospray ionization conditions. The studied oligonucleotide unfolds upon vaporization, loses memory of the solution structure, and explores true gas-phase conformational space. Contrary to our original expectations, the oligonucleotide shows very rich dynamics in three different timescales (multi-picosecond, nanosecond, and sub-millisecond). The shorter timescale dynamics has a quantum mechanical nature and leads to changes in the covalent structure, whereas theother two are of classical origin. Overall, this study suggests that a re-evaluation on our view of the physics of nucleic acids upon vaporization is needed. LB - PUB:(DE-HGF)16 UR - <Go to ISI:>//WOS:000347238800011 C6 - pmid:25417598 DO - DOI:10.1002/anie.201406910 UR - https://juser.fz-juelich.de/record/201331 ER -