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000201679 1001_ $$0P:(DE-HGF)0$$aLeu, Lii-Cherng$$b0$$eCorresponding Author
000201679 245__ $$aOrder–disorder transition in the (1−x)Li $_{2}$ TiO $_{3}$ –xMgO system (0 ≤ x ≤ 0.5)
000201679 260__ $$aLondon$$bRSC Publishing$$c2012
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000201679 520__ $$aThe order–disorder phase transition of magnesium lithium titanate solid–solution (1−x)Li2TiO3–xMgO (0 ≤ x ≤ 0.5) ceramics prepared by conventional solid-state processing has been examined. The phase and structural analysis was carried out using electron diffraction, neutron diffraction and high-resolution transmission electron microscopy. Both electron and neutron diffraction results revealed the onset of an order-to-disorder transition at 0.3 < x < 0.4. Superlattice reflections found in certain regions of x = 0.2 samples and most areas of x = 0.3 samples were caused by a twin structure stabilized by Mg incorporation. Rietveld refinements of neutron diffraction data suggested a random distribution of Mg on the Li 4e sites and equal distribution of Mg on the two Ti 4e sites for x ≤ 0.3. As the Mg content continues to increase, the crystal symmetry transforms from monoclinic to cubic rocksalt. Consequently, the cation ordering on the 8f and 4d sites of the C2/c structure became corrupted and turned into short-range ordering on the 4a sites of a cubic structure with Image ID:c1ra00677k-t1.gif symmetry, resulting in diffuse scattering in electron diffraction patterns.
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000201679 7001_ $$0P:(DE-HGF)0$$aGout, Delphine$$b2
000201679 7001_ $$0P:(DE-HGF)0$$aLetourneau, Steve$$b3
000201679 7001_ $$0P:(DE-HGF)0$$aUbic, Rick$$b4
000201679 773__ $$0PERI:(DE-600)2623224-8$$a10.1039/C1RA00677K$$gVol. 2, no. 4, p. 1598 - 1604$$n4$$p1598 - 1604$$tRSC Advances$$v2$$x2046-2069$$y2012
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