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@ARTICLE{Wellert:202946,
      author       = {Wellert, Stefan and Radulescu, Aurel and Carl, Adrian and
                      Klitzing, Regine von and Gawlitza, Kornelia},
      title        = {{E}volution of {S}ize and {S}tructure during the
                      {P}olymerization {P}rocess: {A} {SANS} {S}tudy on
                      {EG}-{B}ased {M}icrogels},
      journal      = {Macromolecules},
      volume       = {48},
      number       = {14},
      issn         = {1520-5835},
      address      = {Washington, DC},
      publisher    = {Soc.},
      reportid     = {FZJ-2015-05069},
      pages        = {4901 - 4909},
      year         = {2015},
      abstract     = {The present study describes the temporary evolution of size
                      and morphology of thermosensitive and biocompatible microgel
                      particles based on ethylene glycol (EG). P-MeO2MA-co-OEGMA
                      particles were synthesized by precipitation polymerization.
                      The growth of the microgel particles was analyzed at
                      different reaction times using dynamic light scattering
                      (DLS) and small-angle neutron scattering (SANS). The
                      scattering data show the increase of particle size and
                      swelling capability during the polymerization process. After
                      60 min further continuation of the polymerization reaction
                      causes no further change of neither external nor internal
                      particle properties. SANS measurements reveal the formation
                      of a dense core, mainly consisting of cross-linker at an
                      early polymerization state. This is followed by the growth
                      of a loosely packed polymer shell. Nanodomains, observed
                      during the volume phase transition (VPT), as well as a
                      second correlation-length of the network fluctuations arise
                      with progressing polymerization reaction related to the
                      buildup of the shell.},
      cin          = {JCNS (München) ; Jülich Centre for Neutron Science JCNS
                      (München) ; JCNS-FRM-II / Neutronenstreuung ; JCNS-1},
      ddc          = {540},
      cid          = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
                      I:(DE-Juel1)JCNS-1-20110106},
      pnm          = {6G15 - FRM II / MLZ (POF3-6G15) / 6G4 - Jülich Centre for
                      Neutron Research (JCNS) (POF3-623)},
      pid          = {G:(DE-HGF)POF3-6G15 / G:(DE-HGF)POF3-6G4},
      experiment   = {EXP:(DE-MLZ)KWS2-20140101},
      typ          = {PUB:(DE-HGF)16},
      UT           = {WOS:000358823300014},
      doi          = {10.1021/acs.macromol.5b00686},
      url          = {https://juser.fz-juelich.de/record/202946},
}