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000202973 1001_ $$0P:(DE-Juel1)142510$$aBreunig, Katharina$$b0
000202973 245__ $$aProduction of no-carrier-added radiobromine: new nickel selenide target and optimized separation by dry distillation
000202973 260__ $$aBerlin$$bDe @Gruyter$$c2015
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000202973 520__ $$aNickel(II) selenide (NiSe) was investigated as a new high-current target material for cyclotron production of radiobromine, as it contains a higher amount of selenium and has a lower melting point than the widely used Cu2Se. Using a slanted target system, NiSe was successfully tested up to beam currents of 16 μA so far. With regard to the isolation of no-carrier-added (n.c.a.) radiobromide from the target material, an improved dry distillation device with high yields of 76% – 86% was developed. The implementation of a special custom-made quartz funnel decreased the dead volume of the apparatus and a quartz capillary for trapping the radiobromine allowed to concentrate the radioactivity in a small volume of less than 100 μL of 0.1 M NaOH, ready for immediate subsequent radiosyntheses. Thus, the new apparatus improves the handling of the isolation procedure and the radioactive product. The radiochemical purity of the resulting solution of n.c.a. [*Br]bromide was verified by radio-IC where no other species were detected.
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000202973 7001_ $$0P:(DE-Juel1)131849$$aSpahn, Ingo$$b1$$eCorresponding author
000202973 7001_ $$0P:(DE-Juel1)131850$$aSpellerberg, Stefan$$b2
000202973 7001_ $$0P:(DE-Juel1)131816$$aCoenen, Heinrich Hubert$$b3$$ufzj
000202973 773__ $$0PERI:(DE-600)2039575-9$$a10.1515/ract-2014-2366$$gVol. 103, no. 5$$n5$$p397-402$$tRadiochimica acta$$v103$$x2193-3405$$y2015
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