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| Hauptseite > Publikationsdatenbank > Production of no-carrier-added radiobromine: new nickel selenide target and optimized separation by dry distillation > print |
| Hauptseite > Publikationsdatenbank > Production of no-carrier-added radiobromine: new nickel selenide target and optimized separation by dry distillation > print |
| 001 | 202973 | ||
| 005 | 20210129220255.0 | ||
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| 100 | 1 | _ | |a Breunig, Katharina |0 P:(DE-Juel1)142510 |b 0 |
| 245 | _ | _ | |a Production of no-carrier-added radiobromine: new nickel selenide target and optimized separation by dry distillation |
| 260 | _ | _ | |a Berlin |c 2015 |b De @Gruyter |
| 336 | 7 | _ | |a article |2 DRIVER |
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| 520 | _ | _ | |a Nickel(II) selenide (NiSe) was investigated as a new high-current target material for cyclotron production of radiobromine, as it contains a higher amount of selenium and has a lower melting point than the widely used Cu2Se. Using a slanted target system, NiSe was successfully tested up to beam currents of 16 μA so far. With regard to the isolation of no-carrier-added (n.c.a.) radiobromide from the target material, an improved dry distillation device with high yields of 76% – 86% was developed. The implementation of a special custom-made quartz funnel decreased the dead volume of the apparatus and a quartz capillary for trapping the radiobromine allowed to concentrate the radioactivity in a small volume of less than 100 μL of 0.1 M NaOH, ready for immediate subsequent radiosyntheses. Thus, the new apparatus improves the handling of the isolation procedure and the radioactive product. The radiochemical purity of the resulting solution of n.c.a. [*Br]bromide was verified by radio-IC where no other species were detected. |
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| 700 | 1 | _ | |a Spahn, Ingo |0 P:(DE-Juel1)131849 |b 1 |e Corresponding author |
| 700 | 1 | _ | |a Spellerberg, Stefan |0 P:(DE-Juel1)131850 |b 2 |
| 700 | 1 | _ | |a Coenen, Heinrich Hubert |0 P:(DE-Juel1)131816 |b 3 |u fzj |
| 773 | _ | _ | |a 10.1515/ract-2014-2366 |g Vol. 103, no. 5 |0 PERI:(DE-600)2039575-9 |n 5 |p 397-402 |t Radiochimica acta |v 103 |y 2015 |x 2193-3405 |
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