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@ARTICLE{He:203242,
author = {Heß, Volkmar and Matthes, Frank and Bürgler, Daniel and
Monakhov, Kirill Yu. and Besson, Claire and Kögerler, Paul
and Ghisolfi, Alessio and Braunstein, Pierre and Schneider,
Claus M.},
title = {{A}dsorption phenomena of cubane-type tetranuclear
{N}i({II}) complexes with neutral, thioether-functionalized
ligands on {A}u(111)},
journal = {Surface science},
volume = {641},
issn = {0039-6028},
address = {Amsterdam},
publisher = {Elsevier},
reportid = {FZJ-2015-05226},
pages = {210 - 215},
year = {2015},
abstract = {The controlled and intact deposition of molecules with
specific properties onto surfaces is an emergent field
impacting a wide range of applications including catalysis,
molecular electronics, and quantum information processing.
One strategy is to introduce grafting groups functionalized
to anchor to a specific surface. While thiols and disulfides
have proven to be quite effective in combination with gold
surfaces, other S-containing groups have received much less
attention. Here, we investigate the surface anchoring and
organizing capabilities of novel charge-neutral heterocyclic
thioether groups as ligands of polynuclear nickel(II)
complexes. We report on the deposition of a cubane-type
{Ni4} (= [Ni(μ3-Cl)Cl(HL·S)]4) single-molecule magnet from
dichloromethane solution on a Au(111) surface, investigated
by scanning tunneling microscopy, X-ray photoelectron
spectroscopy, and low-energy electron diffraction, both
immediately after deposition and after subsequent
post-annealing. The results provide strong evidence for
partial decomposition of the coordination complex upon
deposition on the Au(111) surface that, however, leaves the
magnetic {Ni4Cl4n} (n = 1 or 2) core intact. Only
post-annealing above 480 K induces further decomposition and
fragmentation of the {Ni4Cl4n} core. The detailed insight
into the chemisorption-induced decomposition pathway not
only provides guidelines for the deposition of
thioether-functionalized Ni(II) complexes on metallic
surfaces but also reveals opportunities to use multidentate
organic ligands decorated with thioether groups as
transporters for highly unstable inorganic structures onto
conducting surfaces, where they are stabilized retaining
appealing electronic and magnetic properties.},
cin = {PGI-6 / JARA-FIT},
ddc = {540},
cid = {I:(DE-Juel1)PGI-6-20110106 / $I:(DE-82)080009_20140620$},
pnm = {522 - Controlling Spin-Based Phenomena (POF3-522)},
pid = {G:(DE-HGF)POF3-522},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000361408800031},
doi = {10.1016/j.susc.2015.06.026},
url = {https://juser.fz-juelich.de/record/203242},
}