TY - JOUR AU - Zhuang, Hao AU - Yang, Nianjun AU - Fu, Haiyuan AU - Zhang, Lei AU - Wang, Chun AU - Huang, Nan AU - Jiang, Xin TI - Diamond Network: Template-Free Fabrication and Properties JO - ACS applied materials & interfaces VL - 7 IS - 9 SN - 1944-8252 CY - Washington, DC PB - Soc. M1 - FZJ-2015-05291 SP - 5384 - 5390 PY - 2015 AB - A porous diamond network with three-dimensionally interconnected pores is of technical importance but difficult to be produced. In this contribution, we demonstrate a simple, controllable, and “template-free” approach to fabricate diamond networks. It combines the deposition of diamond/β-SiC nanocomposite film with a wet-chemical selective etching of the β-SiC phase. The porosity of these networks was tuned from 15 to 68%, determined by the ratio of the β-SiC phase in the composite films. The electrochemical working potential and the reactivity of redox probes on the diamond networks are similar to those of a flat nanocrystalline diamond film, while their surface areas are hundreds of times larger than that of a flat diamond film (e.g., 490-fold enhancement for a 3 μm thick diamond network). The marriage of the unprecedented physical/chemical features of diamond with inherent advantages of the porous structure makes the diamond network a potential candidate for various applications such as water treatment, energy conversion (batteries or fuel cells), and storage (capacitors), as well as electrochemical and biochemical sensing. LB - PUB:(DE-HGF)16 UR - <Go to ISI:>//WOS:000350614600043 DO - DOI:10.1021/am508851r UR - https://juser.fz-juelich.de/record/203324 ER -