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@PHDTHESIS{Jacob:203363,
author = {Jacob, Aurélie},
title = {{T}hermochemical {M}odeling of {L}aves {P}hase {C}ontaining
{F}erritic {S}teels},
volume = {274},
school = {RWTH Aachen},
type = {Dr.},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {FZJ-2015-05316},
isbn = {978-3-95806-070-8},
series = {Schriften des Forschungszentrums Jülich Reihe Energie $\&$
Umwelt / Energy $\&$ Environment},
pages = {200 S.},
year = {2015},
note = {RWTH Aachen, Diss., 2015},
abstract = {For energy technology, development of new materials is
required to be used for boiler and steam turbineswith high
thermal cyclability, creep strength and excellent corrosion
resistance in steam and high temperatures and also at
downtime in water. Crofer 22H, a new kind of steel jointly
developed at Forschungszentrum Juelich and Thyssen Krupp,
has already shown promising results in laboratory tests. The
formation of Laves phase particles improves the material’s
properties such as creep strength while the high Cr-content
of 22 $\%$ provides excellent corrosion resistance.
Unfortunately, the formation of Laves phase competes with
the formation of other phases. In order to further improve
this type of ferritic steels, knowledge of thermodynamics of
the intermetallic systems forming the Laves
phases(Fe,Cr,Si)$_{2}$(Nb,W) is required for the calculation
of phase stability as a function of composition and
temperature. The Calphad method is of great help for the
calculation of phase stability in technical materials. This
kind of calculation is based on thermodynamic databases.
Calculations with the commercial steel database have shown
to be inaccurate since not all considered alloy systems have
been modeled up to now. The present work aims to provide a
thermodynamic optimization of the systems containing Laves
phases. Thermodynamic data of Laves phase containing systems
were obtained by the Calphad method with an optimization of
the sub-systems containing Laves phases. The Calphad method
relies on the input data for the considered system, their
quality and their quantity are of primary importance for the
obtained thermodynamic assessment. In the present work,
several methods have been used in order to provide
consistent thermodynamic calculations of the phase
equilibria. A combined experimental and modeling approach
was chosen to determine the phase equilibria and
thermodynamic properties in the systems Fe-W, Cr-Nb,
Cr-Fe-Nb and Fe-Nb-Si. DFT calculations were done for all
mentioned systems for the determination of the energy of
formation of the compounds through the chosen model. In the
Fe-W system, in addition to the DFT calculations which are
restricted to 0 K, phonon calculations were performed in
order to obtain the temperature dependence of the Gibbs
energies which were used to improve the Calphad modeling.},
cin = {IEK-2},
cid = {I:(DE-Juel1)IEK-2-20101013},
pnm = {111 - Efficient and Flexible Power Plants (POF3-111) /
HITEC - Helmholtz Interdisciplinary Doctoral Training in
Energy and Climate Research (HITEC) (HITEC-20170406)},
pid = {G:(DE-HGF)POF3-111 / G:(DE-Juel1)HITEC-20170406},
typ = {PUB:(DE-HGF)11 / PUB:(DE-HGF)3},
url = {https://juser.fz-juelich.de/record/203363},
}