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@ARTICLE{Peranio:20467,
author = {Peranio, N. and Winkler, M. and Bessas, D. and Aabdin, Z.
and König, J. and Böttner, H. and Hermann, R. and Eibl,
O.},
title = {{R}oom-temperature {MBE} deposition, thermoelectric
properties, and advanced structural characterization of
binary {B}i2{T}e3 and {S}b2{T}e3 thin films},
journal = {Journal of alloys and compounds},
volume = {521},
issn = {0925-8388},
address = {Lausanne},
publisher = {Elsevier},
reportid = {PreJuSER-20467},
pages = {163 - 173},
year = {2012},
note = {The authors gratefully acknowledge financial support by the
German Research Society DFG, priority programme 1386
"Nanostructured Thermoelectric Materials: Theory, Model
Systems and Controlled Synthesis." R.P.H. and D.B.
acknowledge the Advanced Photon Source for provision of
synchrotron radiation beam time and the help of Dr. D.
Robinson during data acquisition at 6-IDD. R. P. H.
acknowledges support from the Helmholtz-University Young
Investigator Group "Lattice Dynamics in Emerging Functional
Materials."},
abstract = {Sb2Te3 and Bi2Te3 thin films were grown at room temperature
on SiO2 and BaF2 substrates using molecular beam epitaxy. A
layer-by-layer growth was achieved such that metallic layers
of the elements with 0.2 nm thickness were deposited. The
layer structure in the as-deposited films was confirmed by
X-ray diffraction and was seen more clearly in Sb2Te3 thin
films. Subsequent annealing was done at 250 degrees C for 2
h and produced the Sb2Te3 and Bi2Te3 crystal structure as
confirmed by high-energy X-ray diffraction. This preparation
process is referred to as nano-alloying and it was
demonstrated to yield single-phase thin films of these
compounds. In the thin films a significant texture could be
identified with the crystal c axis being almost parallel to
the growth direction for Sb2Te3 and tilted by about 30
degrees for Bi2Te3 thin films. Inplane transport properties
were measured for the annealed films at room temperature.
Both films yielded a charge carrier density of about 2.6 x
10(19) cm (3). The Sb2Te3 films were p-type, had a
thermopower of +130 mu V K-1, and surprisingly high
mobilities of 402 cm(2) V-1 s(-1). The Bi2Te3 films were
n-type, showed a thermopower of -153 mu V K-1, and yielded
significantly smaller mobilities of 80 cm(2) V-1 s(-1). The
chemical composition and microstructure of the films were
investigated by transmission electron microscopy (TEM) on
cross sections of the thin films. The grain sizes were about
500 nm for the Sb2Te3 and 250 nm for the Bi2Te3 films. In
the Bi2Te3 thin film, energy-filtered TEM allowed to image a
Bi-rich grain boundary phase, several nanometers thick. This
secondary phase explains the poor mobilities of the Bi2Te3
thin film. With these results the high potential of the
nano-alloying deposition technique for growing films with a
more complex layer architecture is demonstrated. (C) 2012
Elsevier B.V. All rights reserved.},
keywords = {J (WoSType)},
cin = {PGI-4 / JCNS-2 / JARA-FIT},
ddc = {670},
cid = {I:(DE-Juel1)PGI-4-20110106 / I:(DE-Juel1)JCNS-2-20110106 /
$I:(DE-82)080009_20140620$},
pnm = {Grundlagen für zukünftige Informationstechnologien
(FUEK412) / 544 - In-house Research with PNI (POF2-544)},
pid = {G:(DE-Juel1)FUEK412 / G:(DE-HGF)POF2-544},
shelfmark = {Chemistry, Physical / Materials Science, Multidisciplinary
/ Metallurgy $\&$ Metallurgical Engineering},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000300822300029},
doi = {10.1016/j.jallcom.2012.01.108},
url = {https://juser.fz-juelich.de/record/20467},
}