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000021190 1001_ $$0P:(DE-HGF)0$$aSang, X.F.$$b0
000021190 245__ $$aStable carbon isotope ratio analysis of anhydrosugars in biomass burning aerosol particles from source samples
000021190 260__ $$aColumbus, Ohio$$bAmerican Chemical Society$$c2012
000021190 300__ $$a3312 - 3318
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000021190 440_0 $$01865$$aEnvironmental Science and Technology$$v46$$x0013-936X$$y6
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000021190 520__ $$aA new method for stable carbon isotope ratio analysis of anhydrosugars from biomass burning aerosol particle source filter samples was developed by employing Thermal Desorption--2 Dimensional Gas Chromatography--Isotope Ratio Mass Spectrometry (TD-2DGC-IRMS). Compound specific isotopic measurements of levoglucosan, mannosan, and galactosan performed by TD-2DGC-IRMS in a standard mixture show good agreement with isotopic measurements of the bulk anhydrosugars, carried out by Elemental Analyzer--Isotope Ratio Mass Spectrometry (EA-IRMS). The established method was applied to determine the isotope ratios of levoglucosan, mannosan, and galactosan from source samples collected during combustion of hard wood, softwood, and crop residues. δ(13)C values of levoglucosan were found to vary between -25.6 and -22.2‰, being higher in the case of softwood. Mannosan and galactosan were detected only in the softwood samples showing isotope ratios of -23.5‰ (mannosan) and -25.7‰ (galactosan). The isotopic composition of holocellulose in the plant material used for combustion experiments was determined with δ(13)C values between -28.5 and -23.7‰. The difference in δ(13)C of levoglucosan in biomass burning aerosol particles compared to the parent fuel holocellulose was found to be -1.89 (±0.37)‰ for the investigated biomass fuels. Compound specific δ(13)C measurements of anhydrosugars should contribute to an improved source apportionment.
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000021190 650_2 $$2MeSH$$aAerosols
000021190 650_2 $$2MeSH$$aAir Pollutants: analysis
000021190 650_2 $$2MeSH$$aAngiosperms
000021190 650_2 $$2MeSH$$aBiomass
000021190 650_2 $$2MeSH$$aCarbon Isotopes: analysis
000021190 650_2 $$2MeSH$$aGymnosperms
000021190 650_2 $$2MeSH$$aHexoses: analysis
000021190 650_2 $$2MeSH$$aHot Temperature
000021190 650_2 $$2MeSH$$aParticulate Matter: analysis
000021190 650_7 $$00$$2NLM Chemicals$$aAerosols
000021190 650_7 $$00$$2NLM Chemicals$$aAir Pollutants
000021190 650_7 $$00$$2NLM Chemicals$$aCarbon Isotopes
000021190 650_7 $$00$$2NLM Chemicals$$aHexoses
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000021190 7001_ $$0P:(DE-HGF)0$$aGensch, I.$$b1
000021190 7001_ $$0P:(DE-Juel1)129220$$aLaumer, W.$$b2$$uFZJ
000021190 7001_ $$0P:(DE-Juel1)129212$$aKammer, B.$$b3$$uFZJ
000021190 7001_ $$0P:(DE-HGF)0$$aChan, C.Y.$$b4
000021190 7001_ $$0P:(DE-HGF)0$$aEngling, G.$$b5
000021190 7001_ $$0P:(DE-Juel1)16324$$aWahner, A.$$b6$$uFZJ
000021190 7001_ $$0P:(DE-Juel1)VDB50316$$aWissel, H.$$b7$$uFZJ
000021190 7001_ $$0P:(DE-Juel1)4528$$aKiendler-Scharr, A.$$b8$$uFZJ
000021190 773__ $$0PERI:(DE-600)1465132-4$$a10.1021/es204094v$$gVol. 46, p. 3312 - 3318$$p3312 - 3318$$q46<3312 - 3318$$tEnvironmental Science & Technology$$v46$$x0013-936X$$y2012
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