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000021844 084__ $$2WoS$$aChemistry, Organic
000021844 1001_ $$0P:(DE-HGF)0$$aNikishkin, N.I.$$b0
000021844 245__ $$aPalladium-Catalyzed Cross-Coupling of Various Phosphorous Pronucleophiles with Chloropyrazines - Synthesis of Novel An(III)-selective Extractants
000021844 260__ $$aCambridge$$bRoyal Society of Chemistry$$c2012
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000021844 440_0 $$023641$$aOrganic & Biomolecular Chemistry$$v10$$x1477-0520$$y28
000021844 500__ $$aThe authors gratefully acknowledge the financial support from the EU ACSEPT (Actinide reCycling by SEParation and Transmutation) project (FP7 collaborative project 211267).
000021844 520__ $$aPalladium-catalyzed cross-coupling of (di)chloropyrazines with phosphorus pronucleophiles in the presence of a base gave the phosphorylated pyrazines in 81-95% yields. Based on this methodology a series of appropriately functionalized pyrazines was prepared as potential extractants of trivalent cations from highly acidic nuclear waste. A few hydrophilic derivatives exhibited a very good selectivity for Am(3+) over Eu(3+) with separation factors up to 40 at pH 1 at 0.01 mol L(-1) ligand concentration.
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000021844 7001_ $$0P:(DE-HGF)0$$aHuskens, J.$$b1
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000021844 7001_ $$0P:(DE-HGF)0$$aVerboom, W.$$b5
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000021844 8567_ $$uhttp://dx.doi.org/10.1039/C2OB25787D
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