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| Home > Publications database > Palladium-Catalyzed Cross-Coupling of Various Phosphorous Pronucleophiles with Chloropyrazines - Synthesis of Novel An(III)-selective Extractants > print |
| 001 | 21844 | ||
| 005 | 20240708133916.0 | ||
| 024 | 7 | _ | |a pmid:22707012 |2 pmid |
| 024 | 7 | _ | |a 10.1039/C2OB25787D |2 DOI |
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| 041 | _ | _ | |a eng |
| 082 | _ | _ | |a 540 |
| 084 | _ | _ | |2 WoS |a Chemistry, Organic |
| 100 | 1 | _ | |a Nikishkin, N.I. |b 0 |0 P:(DE-HGF)0 |
| 245 | _ | _ | |a Palladium-Catalyzed Cross-Coupling of Various Phosphorous Pronucleophiles with Chloropyrazines - Synthesis of Novel An(III)-selective Extractants |
| 260 | _ | _ | |a Cambridge |b Royal Society of Chemistry |c 2012 |
| 300 | _ | _ | |a 5443 - 5451 |
| 336 | 7 | _ | |a Journal Article |0 PUB:(DE-HGF)16 |2 PUB:(DE-HGF) |
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| 336 | 7 | _ | |a article |2 DRIVER |
| 440 | _ | 0 | |a Organic & Biomolecular Chemistry |x 1477-0520 |0 23641 |y 28 |v 10 |
| 500 | _ | _ | |a The authors gratefully acknowledge the financial support from the EU ACSEPT (Actinide reCycling by SEParation and Transmutation) project (FP7 collaborative project 211267). |
| 520 | _ | _ | |a Palladium-catalyzed cross-coupling of (di)chloropyrazines with phosphorus pronucleophiles in the presence of a base gave the phosphorylated pyrazines in 81-95% yields. Based on this methodology a series of appropriately functionalized pyrazines was prepared as potential extractants of trivalent cations from highly acidic nuclear waste. A few hydrophilic derivatives exhibited a very good selectivity for Am(3+) over Eu(3+) with separation factors up to 40 at pH 1 at 0.01 mol L(-1) ligand concentration. |
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| 700 | 1 | _ | |a Huskens, J. |b 1 |0 P:(DE-HGF)0 |
| 700 | 1 | _ | |a Assenmacher, J. |b 2 |u FZJ |0 P:(DE-Juel1)VDB93843 |
| 700 | 1 | _ | |a Wilden, A. |b 3 |u FZJ |0 P:(DE-Juel1)130438 |
| 700 | 1 | _ | |a Modolo, G. |b 4 |u FZJ |0 P:(DE-Juel1)130383 |
| 700 | 1 | _ | |a Verboom, W. |b 5 |0 P:(DE-HGF)0 |
| 773 | _ | _ | |a 10.1039/c2ob25787d |g Vol. 10, p. 5443 - 5451 |p 5443 - 5451 |q 10<5443 - 5451 |0 PERI:(DE-600)2097583-1 |t Organic & biomolecular chemistry |v 10 |y 2012 |x 1477-0520 |
| 856 | 7 | _ | |u http://dx.doi.org/10.1039/C2OB25787D |
| 856 | 4 | _ | |u https://juser.fz-juelich.de/record/21844/files/FZJ-21844.pdf |y Published under German "Allianz" Licensing conditions on 2012-06-01. Available in OpenAccess from 2013-06-01 |z Published final document. |
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| 914 | 1 | _ | |y 2012 |
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