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@PHDTHESIS{Toscano:2198,
author = {Toscano, Juan},
title = {{I}nfluence of {C}omposition and {P}rocessing on the
{O}xidation {B}ehviour of {MC}r{A}l{Y} {C}oatings for {TBC}
{A}pplications},
volume = {28},
issn = {1866-1793},
school = {RWTH Aachen},
type = {Dr. (Univ.)},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {PreJuSER-2198},
isbn = {978-3-89336-556-2},
series = {Schriften des Forschungszentrums Jülich : Energie $\&$
Umwelt / Energy $\&$ Environment},
pages = {168 S.},
year = {2008},
note = {Record converted from VDB: 12.11.2012; Aachen, RWTH, Diss.,
2008},
abstract = {The adherence of the thermally grown oxide (TGO) to the
bond coat is recognized to be crucial for the lifetime of
thermal barrier coatings (TBC) in aircraft engine and gas
turbine blades. The stability of the system has to be
guaranteed over extended service times (around 25000h) at
high operation temperatures. With this aim, it is necessary
that the TGO is slowgrowing and adherent. This work studies
the influence of different parameters in the oxidation
behavior and scale adherence on MCrAlY-bond coats. For this
purpose, three MCrAlY-coatings were selected and subjected
to oxidation tests at high temperature in the form of TBC
systems, overlay coatings and free-standing coatings. The
first part of the work treats the influence of the chemical
composition on the oxidation behavior of the bond coat. The
second part investigates the influence of non
material-dependent parameters: starting with geometrical
parameters (surface roughness and coating thickness) and
followed by pretreatment/ processing parameters (surface
processing sequence, heat treatment parameters and amount of
O-impurities). Finally, the work deals with the possibility
of defining a critical TGO thickness to failure in EB-PVD
TBC systems. The results demonstrate that not only the
chemical composition of a MCrAlY-coating but also those
geometrical and processing parameters selected can have an
influence on its oxidation behavior and scale adherence. The
studied Co-base coating exhibited better resistance to scale
spallation despite faster oxidation kinetics, apparently
favored by phase stability over a wide temperature range.
Furthermore, it is shown that for a specific material, the
oxidation behavior can be considerably influenced by the
geometrical and processing parameters mentioned above. In
general this influence was achieved due to a variation of
the yttrium reservoir, mobility and/or distribution, which
in turn determined to which extent this element can act at
the surface during oxidation. Only by varying the oxygen
partial pressure of the atmosphere could be obtained scales
with different oxidation kinetics but identical in
morphology and composition. After assessment of these scales
it seemed to be that a critical TGO thickness to failure in
EB-PVD TBC systems exists.},
cin = {IEF-2},
cid = {I:(DE-Juel1)VDB810},
pnm = {Rationelle Energieumwandlung},
pid = {G:(DE-Juel1)FUEK402},
typ = {PUB:(DE-HGF)11 / PUB:(DE-HGF)3},
url = {https://juser.fz-juelich.de/record/2198},
}