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@BOOK{ChogondahalliMuniraju:22244,
author = {Chogondahalli Muniraju, Naveen Kumar},
title = {{C}rystal and spin structure and their relation to physical
properties in some geometrical and spin spiral multiferoics},
volume = {44},
address = {Jülich},
publisher = {Forschungszentrum Jülich GmbH Zentralbibliothek, Verlag},
reportid = {PreJuSER-22244},
isbn = {978-3-89336-802-0},
series = {Schriften des Forschungszentrums Jülich.
Schlüsseltechnologien / Key Technologies},
pages = {III, 190 S.},
year = {2012},
note = {Record converted from VDB: 12.11.2012},
abstract = {The aim of the present work has been to synthesize and to
investigate crystal and spin structure in some geometrical
and spin spiral multiferroics. Multiferroic materials
exhibit two or more ferroic properties such as,
ferroelectricity, ferromagnetism and ferroelasticity. These
materials are considered as prime candidates for future
computer data storage and spintronics. There are several
classes of magnetoelectric multiferroics classified based on
the origin of multiferroicity. The two types of multiferroic
compounds investigated in the present dissertation are,
geometrically frustrated systems including; hexagonal
DyMnO$_{3}$ (hDMO) and orthorhombic HoCrO$_{3}$ (HCO) and
spin spiral systems including wolframite type
Mn$_{0.9}$Co$_{0.1}$WO$_{4}$ (MCoW) and
Mn$_{0.9}$Cu$_{0.1}$WO$_{4}$ (MCuW). The samples were
characterized by macroscopic techniques; specific heat and
magnetization as well as microscopic techniques; x-ray
diffraction and neutron scattering. Polycrystalline samples
of HCO were prepared by solid state reaction method and the
phase purity is confirmed by x-ray diffraction measurements.
From magnetization measurements we determined magnetic
ordering temperature and also an indication of
antiferromagnetic exchange interactions is found. In
isothermal magnetization measurements a hysteretic behavior
was observed indicating the presence of ferromagnetism. Two
magnetic field induced transitions is also found from
isothermal magnetization measurements. The thermal
properties of HCO can be very well described in terms of
lattice, hyperfine and crystal field interaction
contributions. From the specific heat data the contributions
from lattice, hyperfine and crystal field interactions was
determined. The hyperfine field at Ho site and the hyperfine
splitting energy are deduced. Using a Schottky formula for
multiple crystal field levels, five crystal field energies
were computed. Magnetic ordering of both Cr and and Ho
moments in HCO was determined by neutron powder diffraction
(NPD) measurements. The Cr magnetic moments order
antiferromagnetically with a small canting angle about
crystallographic z-direction while the ordering of Ho
moments is a induced type. Ho orders antiferromagnetically
within ab-plane with weak ferromagnetic component along
$\textit{b}$-direction. The thermal variation of Cr and Ho
ordered moments was understood based on molecular field (MF)
theory. The obtained molecular field constants reveals that
Cr–Cr interactions are stronger compared to Ho–Cr
interactions. The lowest crystal field splitting energy
obtained from MF theory is in good agreement with the value
obtained from specific heat and inelastic neutron scattering
(INS) measurements. NPD data also indicated the presence of
spin fluctuations which was confirmed by INS measurements.
From INS data the correlation length of short range ordering
was calculated using Selyakov-Scherrer formula. [...]},
cin = {PGI-4 / JCNS-2 / JARA-FIT},
cid = {I:(DE-Juel1)PGI-4-20110106 / I:(DE-Juel1)JCNS-2-20110106 /
$I:(DE-82)080009_20140620$},
pnm = {Grundlagen für zukünftige Informationstechnologien},
pid = {G:(DE-Juel1)FUEK412},
typ = {PUB:(DE-HGF)3},
url = {https://juser.fz-juelich.de/record/22244},
}