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000022300 0247_ $$2pmid$$apmid:22332882
000022300 0247_ $$2DOI$$a10.1021/ic300042q
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000022300 084__ $$2WoS$$aChemistry, Inorganic & Nuclear
000022300 1001_ $$0P:(DE-HGF)0$$aFielden, J.$$b0
000022300 245__ $$aChiral Hexanuclear Ferric Wheels
000022300 260__ $$aWashington, DC$$bAmerican Chemical Society$$c2012
000022300 300__ $$a2734 - 2736
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000022300 440_0 $$014061$$aInorganic Chemistry$$v51$$x0020-1669$$y5
000022300 500__ $$3POF3_Assignment on 2016-02-29
000022300 500__ $$aWe thank Joost de Groot (Forschungszentrum Julich) and Louise Natrajan (University of Manchester) for help with X-ray diffraction and paramagnetic NMR. Work at the Ames Laboratory was supported by the Department of Energy, Basic Energy Sciences, under Contract DE-AC02-07CH11358.
000022300 520__ $$aThe homochiral iron(III) wheels [Fe(6){(S)-pedea}(6)Cl(6)] and [Fe(6){(R)-pedea)}(6)Cl(6)] [(R)- and (S)-2; pedea = phenylethylaminodiethoxide] exhibit high optical activities and antiferromagnetic exchange. These homochiral products react with each other, producing the centrosymmetric, crystallographically characterized [Fe(6){(S)-pedea}(3){(R)-pedea}(3)Cl(6)] diastereomer [(RSRSRS)-2]. (1)H NMR and UV-vis studies indicate that exchange processes are slow in both homo- and heterochiral systems but that, upon combination, the reaction between (R)- and (S)-2 occurs quickly.
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000022300 650_2 $$2MeSH$$aCircular Dichroism
000022300 650_2 $$2MeSH$$aCrystallography, X-Ray
000022300 650_2 $$2MeSH$$aFerric Compounds: chemistry
000022300 650_2 $$2MeSH$$aMagnetic Resonance Spectroscopy
000022300 650_2 $$2MeSH$$aModels, Molecular
000022300 650_2 $$2MeSH$$aStereoisomerism
000022300 650_7 $$00$$2NLM Chemicals$$aFerric Compounds
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000022300 7001_ $$0P:(DE-HGF)0$$aSpeldrich, M.$$b1
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000022300 7001_ $$0P:(DE-Juel1)VDB12080$$aKögerler, P.$$b3$$uFZJ
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