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000022532 084__ $$2WoS$$aChemistry, Physical
000022532 084__ $$2WoS$$aPhysics, Atomic, Molecular & Chemical
000022532 1001_ $$0P:(DE-HGF)0$$aRosenfeldt, S.$$b0
000022532 245__ $$aPatchy worm-like micelles: solution structure studied by small-angle neutron scattering
000022532 260__ $$aCambridge$$bRSC Publ.$$c2012
000022532 300__ $$a12750 - 12756
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000022532 440_0 $$04916$$aPhysical Chemistry Chemical Physics$$v14$$x1463-9076
000022532 500__ $$aThis work was supported by the German Science Foundation (Collaborative Research Center 840, project A2). We thank the Julich Center of Neutron Scattering (JCNS, Germany) for financial travel support and for providing beamtime at the KWS 1 instrument at FRM II in Munich, Germany.
000022532 520__ $$aTriblock terpolymers exhibit a rich self-organization behavior including the formation of fascinating cylindrical core-shell structures with a phase separated corona. After crystallization-induced self-assembly of polystyrene-block-polyethylene-block-poly(methyl methacrylate) triblock terpolymers (abbreviated as SEMs = Styrene-Ethylene-Methacrylates) from solution, worm-like core-shell micelles with a patchy corona of polystyrene and poly(methyl methacrylate) were observed by transmission electron microscopy. However, the solution structure is still a matter of debate. Here, we present a method to distinguish in situ between a Janus-type (two faced) and a patchy (multiple compartments) configuration of the corona. To discriminate between both models the scattering intensity must be determined mainly by one corona compartment. Contrast variation in small-angle neutron scattering enables us to focus on one compartment of the worm-like micelles. The results validate the existence of the patchy structure also in solution.
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000022532 65017 $$0V:(DE-MLZ)GC-1602-2016$$2V:(DE-HGF)$$aPolymers, Soft Nano Particles and  Proteins$$x1
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000022532 693__ $$0EXP:(DE-MLZ)KWS1-20140101$$1EXP:(DE-MLZ)FRMII-20140101$$5EXP:(DE-MLZ)KWS1-20140101$$6EXP:(DE-MLZ)NL3b-20140101$$aForschungs-Neutronenquelle Heinz Maier-Leibnitz$$eKWS-1: Small angle scattering diffractometer$$fNL3b$$x0
000022532 7001_ $$0P:(DE-HGF)0$$aLüdel, F.$$b1
000022532 7001_ $$0P:(DE-HGF)0$$aSchulreich, C.$$b2
000022532 7001_ $$0P:(DE-HGF)0$$aHellweg, T.$$b3
000022532 7001_ $$0P:(DE-Juel1)VDB4342$$aRadulescu, A.$$b4$$uFZJ
000022532 7001_ $$0P:(DE-HGF)0$$aSchmelz, J.$$b5
000022532 7001_ $$0P:(DE-HGF)0$$aSchmalz, H.$$b6
000022532 7001_ $$0P:(DE-HGF)0$$aHarnau, L.$$b7
000022532 773__ $$0PERI:(DE-600)1476244-4$$a10.1039/c2cp41231d$$gVol. 14, p. 12750 - 12756$$p12750 - 12756$$q14<12750 - 12756$$tPhysical Chemistry Chemical Physics$$v14$$x1463-9076$$y2012
000022532 8567_ $$uhttp://dx.doi.org/10.1039/C2CP41231D
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