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@ARTICLE{Kuhn:23008,
author = {Kuhn, A. and Wilkening, M. and Robben, L. and Choi, J.-Y.
and Tietz, F. and Heitjans, P.},
title = {{L}i {I}on {D}ynamics in {A}l-{D}oped {G}arnet-{T}ype
{L}i7{L}a3{Z}r2{O}12 {C}rystallizing with {C}ubic
{S}ymmetry},
journal = {Zeitschrift für Physikalische Chemie},
volume = {226},
issn = {0942-9352},
address = {München},
publisher = {Oldenbourg},
reportid = {PreJuSER-23008},
pages = {525-537},
year = {2012},
note = {We thank Marc Krey for the ICP-OES analysis. Financial
support by the Federal Ministry of Education and Science
(BMBF) within the framework of the "Kompetenzverbund Nord"
and by the Deutsche Forschungsgemeinschaft (DFG) via the
Research Unit 1277 (molife) is gratefully acknowledged. A.
K. acknowledges support by the Studienstiftung des deutschen
Volkes e.V.},
abstract = {Lithium-ion dynamics in the garnet-type solid electrolyte
"Li7La3Zr2O12" (LLZ) crystallizing with cubic symmetry was
probed by means of variable-temperature Li-7 NMR
spectroscopy and ac impedance measurements. Li jump rates of
an Al-containing sample follow Arrhenius behavior being
characterized by a relatively high activation energy of
0.54(3) eV and a pre-exponential factor of 2.2(5) x 10(13)
s(-1). The results resemble those which were quite recently
obtained for an Al-free LLZ sample crystallizing, however,
with tetragonal symmetry. Hence, most likely, the
significantly higher Li conductivity previously reported for
a cubic LLZ sample cannot be ascribed solely to the slight
structural distortions accompanying the change of the
crystal symmetry. Here, even Al impurities, acting as
stabilizer for the cubic polymorph at room temperature, do
not lead to the high ion conductivity reported previously.},
keywords = {J (WoSType)},
cin = {IEK-1},
ddc = {540},
cid = {I:(DE-Juel1)IEK-1-20101013},
pnm = {Rationelle Energieumwandlung},
pid = {G:(DE-Juel1)FUEK402},
shelfmark = {Chemistry, Physical},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000307315500014},
doi = {10.1524/zpch.2012.0250},
url = {https://juser.fz-juelich.de/record/23008},
}