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@ARTICLE{Choe:26893,
author = {Choe, B. J. and Jeong, D.-G. and Park, K. S. and
Schlesinger, R. and Labahn, J. and Hofmann, K. P. and
Büldt, G.},
title = {{P}reliminary {X}-ray characterization of the ribonuclease
{P} ({C}5 protein) from {E}scherichia coli : expression,
crystallization and cryoconditions},
journal = {Acta crystallographica / D},
volume = {59},
issn = {0907-4449},
address = {Copenhagen},
publisher = {Munksgaard},
reportid = {PreJuSER-26893},
pages = {350 - 352},
year = {2003},
note = {Record converted from VDB: 12.11.2012},
abstract = {The gene for Escherichia coli ribonuclease P (RNase P)
protein (also known as C5 protein) and its mutant C5-C113A
have been expressed as GST fusion proteins in E. coli at a
high level. After cleavage of the fusion protein, highly
purified functional C5 protein is obtained that can be
crystallized with 2.5-2.6 M
(NH(4))(2)HPO(4)/(NH(4))H(2)PO(4) pH 7.0 at room
temperature. These crystals are suitable for X-ray analysis,
belong to the space group P3(1)21 or P3(2)21 (unit-cell
parameters a = b = 66.67, c = 142.09 A) and diffract to 2.9
A at 100 K using sorbitol and glycerol as cryoprotectants.
For three molecules in the asymmetric unit a V(M) of 2.17
A(3) Da(-1) was calculated.},
keywords = {Amino Acid Substitution / Cryoprotective Agents: chemistry
/ Crystallization / Crystallography, X-Ray /
Endoribonucleases: chemistry / Endoribonucleases: genetics /
Endoribonucleases: metabolism / Escherichia coli: enzymology
/ Escherichia coli Proteins / Glutathione Transferase:
genetics / Glycerol: chemistry / RNA, Catalytic: chemistry /
RNA, Catalytic: genetics / RNA, Catalytic: metabolism /
Recombinant Fusion Proteins: biosynthesis / Recombinant
Fusion Proteins: genetics / Ribonuclease P /
Ribonucleoproteins: chemistry / Ribonucleoproteins: genetics
/ Ribonucleoproteins: metabolism / Sorbitol: chemistry /
Cryoprotective Agents (NLM Chemicals) / Escherichia coli
Proteins (NLM Chemicals) / RNA, Catalytic (NLM Chemicals) /
Recombinant Fusion Proteins (NLM Chemicals) /
Ribonucleoproteins (NLM Chemicals) / Sorbitol (NLM
Chemicals) / Glycerol (NLM Chemicals) / Glutathione
Transferase (NLM Chemicals) / Endoribonucleases (NLM
Chemicals) / Ribonuclease P (NLM Chemicals) / ribonuclease
P, E coli (NLM Chemicals) / J (WoSType)},
cin = {IBI-2},
ddc = {570},
cid = {I:(DE-Juel1)VDB58},
pnm = {Neurowissenschaften},
pid = {G:(DE-Juel1)FUEK255},
shelfmark = {Biochemical Research Methods / Biochemistry $\&$ Molecular
Biology / Biophysics / Crystallography},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:12554950},
UT = {WOS:000180641900020},
doi = {10.1107/S0907444902020784},
url = {https://juser.fz-juelich.de/record/26893},
}