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000276170 1001_ $$0P:(DE-Juel1)130905$$aRadulescu, Aurel$$b0$$eCorresponding author
000276170 245__ $$aMorphology of crystalline–amorphous olefin block copolymers in solution characterized by small-angle neutron scattering and microscopy
000276170 260__ $$aCopenhagen$$bMunksgaard$$c2015
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000276170 520__ $$aThe single-chain properties and self-assembly behavior in dilute solution of olefin block copolymers obtained by chain-shuttling technology and consisting of alternating crystallizable and amorphous ethylene/1-octene blocks were investigated by pinhole and focusing small-angle neutron scattering techniques, optical microscopy in bright-field and crossed-polarizer modes, and differential scanning calorimetry. The complex hydrocarbon soluble (precipitant free) macro-aggregates formed with decreasing temperature are characterized by spherulitic textures. The spherulites yield, on one hand, a morphology that depends on the chain structure properties and, on the other hand, multiple structural levels with a hierarchical organization that ranges from 10 Å up to tens of micrometres. This morphology displays peculiarities dictated by the polydisperse character of these materials.
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000276170 7001_ $$0P:(DE-HGF)0$$aGoerigk, Günter$$b1
000276170 7001_ $$0P:(DE-HGF)0$$aFetters, Lewis$$b2
000276170 7001_ $$0P:(DE-Juel1)130917$$aRichter, Dieter$$b3$$ufzj
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