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| 100 | 1 | _ | |a Radulescu, Aurel |0 P:(DE-Juel1)130905 |b 0 |e Corresponding author |
| 245 | _ | _ | |a Morphology of crystalline–amorphous olefin block copolymers in solution characterized by small-angle neutron scattering and microscopy |
| 260 | _ | _ | |a Copenhagen |c 2015 |b Munksgaard |
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| 520 | _ | _ | |a The single-chain properties and self-assembly behavior in dilute solution of olefin block copolymers obtained by chain-shuttling technology and consisting of alternating crystallizable and amorphous ethylene/1-octene blocks were investigated by pinhole and focusing small-angle neutron scattering techniques, optical microscopy in bright-field and crossed-polarizer modes, and differential scanning calorimetry. The complex hydrocarbon soluble (precipitant free) macro-aggregates formed with decreasing temperature are characterized by spherulitic textures. The spherulites yield, on one hand, a morphology that depends on the chain structure properties and, on the other hand, multiple structural levels with a hierarchical organization that ranges from 10 Å up to tens of micrometres. This morphology displays peculiarities dictated by the polydisperse character of these materials. |
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