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@ARTICLE{Laptev:276222,
author = {Laptev, Alexander and Daudt, Natália F. and Guillon,
Olivier and Bram, Martin},
title = {{I}ncreased {S}hape {S}tability and {P}orosity of {H}ighly
{P}orous {I}njection-{M}olded {T}itanium {P}arts},
journal = {Advanced engineering materials},
volume = {17},
number = {11},
issn = {1438-1656},
address = {Weinheim},
publisher = {Wiley-VCH Verl.},
reportid = {FZJ-2015-06687},
pages = {1579 - 1587},
year = {2015},
abstract = {Highly porous titanium parts in three different shapes
(conical, cylindrical, and semi-cylindrical) were produced
using metal injection molding (MIM) and the space holder
technique. Potassium chloride (KCl) powder was used as a
temporary space holder material. The frequently used
extraction of the KCl space holder by dissolution in warm
water was replaced with sublimation from the solid state
during vacuum sintering. This improvement enabled highly
porous titanium parts to be manufactured by MIM without the
frequently observed sample collapse or extensive shape
distortion. Final porosities of $55–60\%$ were achieved,
which is close to the recommended value for porous spinal
titanium implants, making improved method attractive for
implant manufacturing applications. An additional advantage
of removing the space holder by sublimation is that the
time-consuming salt leaching step can be omitted. A
systematic study of sample configuration, porosity change,
microstructure, and impurity uptake was conducted and the
sintering cycle was optimized.},
cin = {IEK-1 / JARA-ENERGY},
ddc = {540},
cid = {I:(DE-Juel1)IEK-1-20101013 / $I:(DE-82)080011_20140620$},
pnm = {899 - ohne Topic (POF3-899)},
pid = {G:(DE-HGF)POF3-899},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000367538600009},
doi = {10.1002/adem.201500061},
url = {https://juser.fz-juelich.de/record/276222},
}